2-氯-1-(4-异丁基苯基)丙酮合成路线 (共 7 条)
反应条件
lithium chloride; copper dichloride in N,N-dimethyl-formamide T=80°C; 3 h;
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Belli, Aldo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2575 - 2582
反应条件
aluminium trichloride in 1,2-dichloro-ethane 6 h; Ambient temperature;
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
反应条件
1: 1.) propylene oxide; 2.) NaOH / 1.) MeOH, irradiation, pH neutral; 2.) MeOH, reflux, 2 h 2: 85 percent / Br2 / CCl4 / 1 h 3: 55 percent / propylene oxide / H2O; acetone / Irradiation; pH neutral View Scheme
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
反应条件
methyloxirane in water; acetone IrradiationpH neutral;
参考文献
Tetrahedron, , vol. 50, # 4 p. 1243 - 1260
反应条件
water; methyloxirane in acetone 3 h; Irradiation;
参考文献
Sonawane, Harikisan R.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron Letters, 1990 , vol. 31, # 51 p. 7495 - 7496
反应条件
methyloxirane in water; acetone IrradiationpH neutral;
参考文献
Tetrahedron, , vol. 50, # 4 p. 1243 - 1260
反应条件
1: 1.) propylene oxide; 2.) NaOH / 1.) MeOH, irradiation, pH neutral; 2.) MeOH, reflux, 2 h
2: 85 percent / Br2 / CCl4 / 1 h
View Scheme
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260