potassium carbonate; thiophenol in acetonitrile
T=50°C;
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: 74 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
2: 90 percent / PhSH; potassium carbonate / acetonitrile / 50 °C
View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: 97 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
2: 74 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
3: 90 percent / PhSH; potassium carbonate / acetonitrile / 50 °C
View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: 74 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
2: 90 percent / PhSH; potassium carbonate / acetonitrile / 50 °C
View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
