三甲基硅氧基乙烯基二甲基甲醇合成路线 (共 3 条)
反应条件
in diethyl ether
2 h; Ambient temperature;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 71 - 88
反应条件
oxygen O2, singlet in methanol
T=40°C; 0.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Dubac, J.; Laporterie, A.; Iloughmane, H.; Pillot, J. P.; Deleris, G.; Dunogues, J.
Journal of Organometallic Chemistry, 1985 , vol. 281, p. 149 - 162
反应条件
1: 70 percent / Mg / tetrahydrofuran / Ambient temperature
2: 66 percent Spectr. / singlet O2 / methanol / 0.5 h / 40 °C / Irradiation
View Scheme
参考文献
Dubac, J.; Laporterie, A.; Iloughmane, H.; Pillot, J. P.; Deleris, G.; Dunogues, J.
Journal of Organometallic Chemistry, 1985 , vol. 281, p. 149 - 162