6-(三苯甲基)巯基正己酸合成路线 （共 5 条）
反应条件
1: triphenylmethanethiol With sodium methylate in methanol; acetonitrile 0.25 h; 2: 6-bromo-n-caproic acid in tetrahydrofuran; methanol; acetonitrile T=20°C; 18 h; Further stages.;
参考文献
Mays, Jared R.; Restituyo, Jose A.; Katzenberger, Rebeccah J.; Wassarman, David A.; Rajski, Scott R.
Tetrahedron Letters, 2007 , vol. 48, # 26 p. 4579 - 4583
反应条件
1: 70 percent / conc. HBr, conc. H2SO4 / 10 h / Heating 2: 66 percent / K2CO3 / ethanol / 12 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1391 - 1403
反应条件
lithium hydroxide hydrate in methanol T=40°C; 6 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 17 p. 6587 - 6595
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.33 h / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: lithium hydroxide hydrate / methanol / 6 h / 40 °C / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 17 p. 6587 - 6595
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.33 h / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: lithium hydroxide hydrate / methanol / 6 h / 40 °C / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 17 p. 6587 - 6595
