1: 60 °C / Irradiation
2: 79 percent / lithium aluminium hydride / tetrahydrofuran / 20 °C
View Scheme
参考文献
Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Yin, Ping
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , p. 3925 - 3932
Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Yin, Ping
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , p. 3925 - 3932
1: 1,2-bis(phosphino)benzene With sodium in tetrahydrofuran
48 h;
2: methyl iodide in tetrahydrofuran
T=-78 - 20°C; Further stages. Title compound not separated from byproducts.;
参考文献
Chatterjee; George; Salem; Willis
Journal of the Chemical Society, Dalton Transactions, 2001 , # 12 p. 1890 - 1896
1: 1,2-bis(phosphino)benzene With n-butyllithium in tetrahydrofuran
Metallation;
2: methyl iodide in tetrahydrofuran
Methylation; Further stages.;
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830