三异丙基甲硅烷基三氟甲烷磺酸盐合成路线 （共 52 条）
参考文献
Tetrahedron Letters, , vol. 22, # 36 p. 3455 - 3458
反应条件
in dichloromethane T=0°C; 2 h;
参考文献
Synthesis, , # 7 p. 744 - 746
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 4 p. 1039 - 1048
Tetrahedron Letters, , vol. 28, # 49 p. 6191 - 6194
反应条件
methyllithium; lithium bromide 1.) THF, Et2O, -78 deg C, 3 h, 2.) THF, Et2O, 20 deg C, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rubin, Yves; Lin, Sophia S.; Knobler, Carolyn B.; Anthony, John; Boldi, Armen M.; Diederich, Francois
Journal of the American Chemical Society, 1991 , vol. 113, # 18 p. 6943 - 6949
反应条件
1: cyclohexylacetylene With tBuOOLi; lithium hexamethyldisilazane in tetrahydrofuran; toluene T=-78 - 0°C; 2.5 h; 2: tri-isopropylsylil trifluoromethane sulfonate With tBuOOLi; lithium hexamethyldisilazane in tetrahydrofuran; toluene T=-78 - 0°C;
参考文献
Sun, Jianwei; Keller, Valerie A.; Meyer, S. Todd; Kozmin, Sergey A.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 5 p. 839 - 842
反应条件
1H-imidazole in N,N-dimethyl-formamide
参考文献
Markwalder, Jay A.; Christ, David D.; Mutlib, Abdul; Cordova, Beverly C.; Klabe, Ronald M.; Seitz, Steven P.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 5 p. 619 - 622
反应条件
2,6-dimethylpyridine
参考文献
Markwalder, Jay A.; Christ, David D.; Mutlib, Abdul; Cordova, Beverly C.; Klabe, Ronald M.; Seitz, Steven P.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 5 p. 619 - 622
反应条件
2,6-dimethylpyridine in dichloromethane T=0°C; 2 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP1911738 A1, 2008 ;
Location in patent: Page/Page column 35 ;
反应条件
in water; N,N-dimethyl-formamide
参考文献
Eli Lilly and Company
Patent: US6284756 B1, 2001 ;
US 6284756 B1
反应条件
1: Et3N 2: s-BuLi View Scheme
参考文献
Martin, Stephen F.; Barr, Kenneth J.; Smith, Dudley W.; Bur, Scott K.
Journal of the American Chemical Society, 1999 , vol. 121, # 30 p. 6990 - 6997
