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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
805236-74-2
合成路线
（共 9 条）
805236-74-2
→
反应条件
3335-98-6
N-苯基吲哚酮
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: polyphosphoric acid / 3 h / 95 °C View Scheme
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
28721-09-7
10-甲氧卡马西平
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: 70 percent / polyphosphoric acid / 3 h / 95 °C 3: 81 percent / p-TsOH / methanol / 5 h / Heating 4: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C 5: AcOH / 7 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
28721-07-5
奥卡西平
反应条件
1.1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2.1: polyphosphoric acid / 3 h / 95 °C 3.1: 97 percent / aq. NaOH / 6 h / 100 °C 4.1: 98 percent / dimethylformamide / 4 h / 24 °C 5.1: 98 percent / Et3N; DMAP / CH2Cl2 / 3.5 h / 20 - 40 °C 6.1: 95 percent / hydrogen / Pd/C / methanol / 3 h / 30 °C 7.1: 40 percent / polyphosphoric acid / toluene / 11 h / 110 °C 8.1: aq. Na2CO3 / methanol; H2O / 0.5 h / 23 °C 9.1: CH2Cl2 / 17 h / 25 °C 9.2: 70 percent / H2O View Scheme
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
70172-33-7
苯胺苯乙酸
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: polyphosphoric acid / 3 h / 95 °C 3: 97 percent / aq. NaOH / 6 h / 100 °C 4: acid / pH 2 View Scheme
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
353497-35-5
反应条件
sodium hydroxide in methanol T=25°C; 24 h;
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
353497-31-1
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: 70 percent / polyphosphoric acid / 3 h / 95 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
805236-74-2
→
反应条件
4698-11-7
10-甲氧基亚氨基芪
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: 70 percent / polyphosphoric acid / 3 h / 95 °C 3: 81 percent / p-TsOH / methanol / 5 h / Heating 4: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 27 p. 5275 - 5278
805236-74-2
→
反应条件
21737-58-6
10,11-二氢-5H-二苯并[b,f]氮杂革-10-酮
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: polyphosphoric acid / 3 h / 95 °C 3: 97 percent / aq. NaOH / 6 h / 100 °C 4: 98 percent / dimethylformamide / 4 h / 24 °C 5: 98 percent / Et3N; DMAP / CH2Cl2 / 3.5 h / 20 - 40 °C 6: 95 percent / hydrogen / Pd/C / methanol / 3 h / 30 °C 7: 40 percent / polyphosphoric acid / toluene / 11 h / 110 °C 8: aq. Na2CO3 / methanol; H2O / 0.5 h / 23 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
805236-74-2
→
反应条件
731851-88-0
反应条件
1.1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2.1: polyphosphoric acid / 3 h / 95 °C 3.1: 97 percent / aq. NaOH / 6 h / 100 °C 4.1: nBuLi / tetrahydrofuran 4.2: 38 percent / tetrahydrofuran / 2 h / -10 °C View Scheme
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
