4-(氰基甲基)-苯甲酰氯(9ci)合成路线 （共 7 条）
反应条件
thionyl chloride in N,N-dimethyl-formamide; benzene
1 h; Heating;
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
反应条件
1: 79 percent / H2O / 12 h / Heating
2: SOCl2 / benzene / 24 h / Heating
View Scheme
参考文献
Former, Carsten; Klaerner, Gerrit; Wagner, Manfred; Muellen, Klaus
Advanced Synthesis and Catalysis, 1998 , vol. 340, # 4 p. 367 - 374
反应条件
1: benzene / Heating
2: 46 percent / POCl3 / benzene / Heating
3: 55 percent / 10 percent aq. NaOH / ethanol / Heating
View Scheme
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
反应条件
1: benzene / Heating
2: POCl3 / benzene / Heating
3: 10 percent aq. NaOH / ethanol / Heating
View Scheme
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
反应条件
1: benzene / Heating
2: POCl3 / benzene / Heating
3: 10 percent aq. NaOH / ethanol / Heating
View Scheme
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
反应条件
1: benzene / Heating
2: POCl3 / benzene / Heating
3: 26 percent / 10 percent aq. NaOH / ethanol / Heating
4: 40 percent / diethyl ether / 0 °C
View Scheme
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
反应条件
1: benzene / 16 h / Heating
2: 53 percent / POCl3 / benzene / 2 h / Heating
3: 65 percent / 10 percent aq. NaOH / ethanol / 1 h / Heating
4: 45 percent / diethyl ether / 2 h / 0 °C
View Scheme
参考文献
Shridhar, D. R.; Ram, Bhagat; Sarma, C. R.; Krishna, R. R.; Singh, P. P.; Rao, C. Seshagiri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, p. 891 - 893
