4-甲基-2-间甲苯基吡啶合成路线 (共 5 条)
反应条件
selenium(IV) oxide in pyridine
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
72 h; Inert atmosphereReflux;
参考文献
Sharp Kabushiki Kaisha
Patent: EP2275494 A1, 2011 ;
Location in patent: Page/Page column 24 ;
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0)
Suzuki coupling reaction;
参考文献
Jung, Sungouk; Kang, Youngjin; Kim, Hyung-Sun; Kim, Yun-Hi; Lee, Chang-Lyoul; Kim, Jang-Joo; Lee, Sung-Koo; Kwon, Soon-Ki
European Journal of Inorganic Chemistry, 2004 , # 17 p. 3415 - 3423
反应条件
1: concd. hydrochloric acid, sodium nitrite; sodium carbonate / H2O / 4 °C
2: hydrogen chloride / 100 °C
View Scheme
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031
反应条件
hydrogenchloride
T=100°C;
参考文献
Chatterjea, J. N.; Shaw, S. C.; Prasad, Y.; Singh, R. P.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1028 - 1031