3,4-二氢-3,3-二甲基-(9ci)-2(1h)-喹噁啉酮合成路线 （共 11 条）
反应条件
carbon monoxide; O,O-diethyl O-p-nitrophenyl phosphorothioate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=70°C; P=3040.2 Torr;
参考文献
Organic letters, , vol. 4, # 8 p. 1339 - 1342
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=190°C; 0.1 h; microwave irradiation;
参考文献
Kamila, Sukanta; Biehl, Edward R.
Heterocycles, 2006 , vol. 68, # 9 p. 1931 - 1939
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane T=10°C; overnight;
参考文献
Lai, John T.
Synthesis, 1982 , # 1 p. 71 - 74
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane T=10°C; overnight;
参考文献
Lai, John T.
Synthesis, 1982 , # 1 p. 71 - 74
反应条件
sodium hydroxide in chloroform
反应条件
potassium phosphate; copper(l) chloride; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=110°C; Ullmann reaction; 24 h; Inert atmosphereSealed tube;
参考文献
Tanimori, Shinji; Inaba, Ushio; Kato, Yoshihiro; Ura, Haruna; Kashiwagi, Hiroaki; Nishimura, Takeshi; Kirihata, Mitsunori
Research on Chemical Intermediates, 2014 , vol. 40, # 6 p. 2157 - 2164
反应条件
1: -20 °C / |Molecular sieve 2: carbon monoxide; bis(dibenzylideneacetone)-palladium(0) / acetonitrile / 70 °C / 3040.2 Torr View Scheme
参考文献
Tetrahedron, , vol. 69, # 4 p. 1403 - 1416
反应条件
1: triphenylphosphine / diethyl ether 2: -20 °C / |Molecular sieve 3: carbon monoxide; bis(dibenzylideneacetone)-palladium(0) / acetonitrile / 70 °C / 3040.2 Torr View Scheme
参考文献
Tetrahedron, , vol. 69, # 4 p. 1403 - 1416
反应条件
potassium hydroxide; ethanol
参考文献
Gazzetta Chimica Italiana, , vol. 59, p. 824
参考文献
Gazzetta Chimica Italiana, , vol. 59, p. 824
