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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
80639-39-0
合成路线
（共 10 条）
846601-41-0
→
反应条件
80639-39-0
反应条件
copper diacetate; palladium diacetate; potassium carbonate in toluene 24 h; Inert atmosphereReflux;
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
162330-95-2
→
反应条件
80639-39-0
反应条件
copper diacetate; palladium diacetate; potassium carbonate in toluene 24 h; Inert atmosphereReflux;
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
3490-06-0
N-甲基-2-(3,4-二甲氧基苯基)乙胺
→
反应条件
80639-39-0
反应条件
1: bromine / acetic acid 2: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
1357480-92-2
→
反应条件
80639-39-0
反应条件
1: potassium carbonate / methanol; water / 2 h / 20 °C 2: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
13230-71-2
→
反应条件
80639-39-0
反应条件
1.1: iodine / dichloromethane / 15 h / 20 °C 2.1: potassium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 - 5 °C / Inert atmosphere 2.2: 17 h / 20 °C / Inert atmosphere; Reflux 3.1: potassium carbonate / methanol; water / 2 h / 20 °C 4.1: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
154138-43-9
→
反应条件
80639-39-0
反应条件
1.1: potassium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 - 5 °C / Inert atmosphere 1.2: 17 h / 20 °C / Inert atmosphere; Reflux 2.1: potassium carbonate / methanol; water / 2 h / 20 °C 3.1: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
75767-96-3
→
反应条件
80639-39-0
反应条件
1: 2.) 10percent aq. HCl / 1.) 90 deg C, 8 h, 2.) RT, 1 h 2: 42 percent / t-BuOK / dimethylsulfoxide / 0.5 h / Irradiation View Scheme
参考文献
Fidalgo, Jesus; Castedo, Luis; Dominguez, Domingo
Heterocycles, 1994 , vol. 39, # 2 p. 581 - 590
141438-33-7
→
反应条件
80639-39-0
反应条件
sec.-butyllithium; lithium bromide 1) THF, 30 min, RT, 2) THF, -78 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
141438-48-4
→
反应条件
80639-39-0
反应条件
1: LiAlH4 / 24 h / Heating 2: ammonium sulfate / 24 h / Heating 3: 1) LiBr, 2) sec-butyllithium / 1) THF, 30 min, RT, 2) THF, -78 deg C, 10 min View Scheme
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
80639-39-0
→
反应条件
80639-40-3
反应条件
air
参考文献
Kessar, Satinder V.; Singh, Paramjit; Chawla, Ravinder; Kumar, Pawan
Journal of the Chemical Society, Chemical Communications, 1981 , # 20 p. 1074 - 1075
