反应条件
in tetrahydrofuran THF was condensed onto K(HRu3(CO)11) at -78°C under N2, ca. 1 atm of CO was expanded, soln. was warmed to room temp., stirred vigorously for 3 weeks; CO was removed, white solid from walls of the vessel proved to be KH (according to its X-ray powder diffracion pattern), THF soln. was pipetted off, residue was extd. with THF, ext. contained only Ru3(CO)12 (IR spectral identification);
参考文献
Bricker, Jeffery C.; Payne, Martin W.; Shore, Sheldon G.
Organometallics, 1987 , vol. 6, p. 2545 - 2547