1.1: NaH / tetrahydrofuran / 0.17 h / 0 °C
1.2: tetrahydrofuran / 6 h / 20 °C
2.1: 1.32 g / K2CO3 / H2O / 2 h / 80 °C
3.1: 85 percent / DIBAL-H / CH2Cl2 / 2 h / -78 °C
View Scheme
参考文献
Tong, Rongbiao; McDonald, Frank E.; Fang, Xikui; Hardcastle, Kenneth I.
Synthesis, 2007 , # 15 p. 2337 - 2342
