2,6,10,10-四甲基-1-氧杂螺[4.5]癸-2,6-二烯-8-酮合成路线 （共 3 条）
反应条件
sulfuric acid in dichloromethane
0.5 h; Yield given;
参考文献
Shibagaki, Makoto; Shibata, Saizo; Kaneko, Hajime
Agricultural and Biological Chemistry, 1981 , vol. 45, # l2 p. 2911 - 2914
反应条件
1: 82 percent / Li / tetrahydrofuran / 5 h / Ambient temperature
2: 0.1 N HCl / tetrahydrofuran / 20 h / Ambient temperature
3: 0.1 N H2SO4 / CH2Cl2 / 0.5 h
View Scheme
参考文献
Shibagaki, Makoto; Shibata, Saizo; Kaneko, Hajime
Agricultural and Biological Chemistry, 1981 , vol. 45, # l2 p. 2911 - 2914
反应条件
1: 0.1 N HCl / tetrahydrofuran / 20 h / Ambient temperature
2: 0.1 N H2SO4 / CH2Cl2 / 0.5 h
View Scheme
参考文献
Shibagaki, Makoto; Shibata, Saizo; Kaneko, Hajime
Agricultural and Biological Chemistry, 1981 , vol. 45, # l2 p. 2911 - 2914
