1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol
T=20°C; Tamao-Kumada oxidation; 12 h;
参考文献
Angelaud, Remy; Landais, Yannick
Tetrahedron, 2000 , vol. 56, # 14 p. 2025 - 2036
反应条件
lithium bromide in tetrahydrofuran; chloroform
T=20°C; 15 h;
参考文献
Gable; Shanmugham; White
Canadian Journal of Chemistry, 2000 , vol. 78, # 6 p. 704 - 707
反应条件
indium in water
T=20°C; Barbier-type allylation;
参考文献
Vilaivan, Tirayut; Winotapan, Chutima; Shinada, Tetsuro; Ohfune, Yasufumi
Tetrahedron Letters, 2001 , vol. 42, # 51 p. 9073 - 9076
反应条件
1: With indium in tetrahydrofuran
T=50°C; 5 h;
2: With hydrogenchloride in tetrahydrofuran
Further stages.;
参考文献
Hirashita, Tsunehisa; Hayashi, Yousuke; Mitsui, Kazuma; Araki, Shuki
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1309 - 1313
反应条件
1: allyltributylstannane; benzaldehyde With boron trifluoride diethyl etherate in toluene
T=-35°C; Inert atmosphere;
2: phenylacetylene With tris(pentafluorophenyl)-borane in toluene
3 h; Inert atmosphere; SolventTemperatureReagent/catalyst;
参考文献
Ghosh, Banibrata; Amado-Sierra, Maria Del Rosario I.; Holmes, Daniel; Maleczka, Robert E.
Organic Letters, 2014 , vol. 16, # 9 p. 2318 - 2321
反应条件
tetrakis(triphenylphosphine) palladium(0); (C2H5)2AlSnClF2 in hexane; dichloromethane
T=20°C; 2 h;
参考文献
Matsubara, Seijiro; Wakamatsu, Kuni; Morizawa, Yoshitomi; Tsuboniwa, Noriyuki; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 4 p. 1196 - 1199
反应条件
2,2,2-trifluoroethanol in tetrahydrofuran
T=60°C; 3.5 h;
参考文献
Asao, Naoki; Abe, Noriko; Tan, Zheng; Maruoka, Keiji
Synlett, 1998 , # 4 p. 377 - 378
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; (S,S)-N,N-bis(α-methylbenzyl)formamide in various solvent(s)
T=-78°C; 168 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iseki, Katsuhiko; Mizuno, Shin; Kuroki, Yoshichika; Kobayashi, Yoshiro
Tetrahedron Letters, 1998 , vol. 39, # 18 p. 2767 - 2770
反应条件
water; scandium tris(trifluoromethanesulfonate) in nitromethane
T=20°C; Addition; 1.5 h;
参考文献
Akiyama, Takahiko; Iwai, Junko; Sugano, Megumi
Tetrahedron, 1999 , vol. 55, # 24 p. 7499 - 7508
反应条件
1: styrene With oxygen in dichloromethane
T=-78°C; ozonolysis; 0.166667 h;
2: allyl bromide With ammonium chloride; zinc in tetrahydrofuran
T=0°C; Rearrangement; 0.25 h;
参考文献
Schloss, Jeffrey D.; Paquette, Leo A.
Synthetic Communications, 1998 , vol. 28, # 15 p. 2887 - 2892
