1-苯基-3-丁烯-1-醇合成路线 (共 285 条)
反应条件
4 A molecular sieve; tin(ll) chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in dichloromethane
T=20°C;
参考文献
Roy, Ujjal Kanti; Roy, Sujit
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7177 - 7180
反应条件
potassium fluoride; aluminium in water
T=20°C; Barbier type alkylation; 18 h;
参考文献
Yuan, Shizhen; Liu, Jin; Xu, Ling; Zhu, Shaofeng
Chinese Journal of Chemistry, 2010 , vol. 28, # 4 p. 578 - 582
反应条件
chromium dichloride in N,N-dimethyl-formamide
2.6 h; Ambient temperature;
参考文献
Hiyama, Tamejiro; Okude, Yoshitaka; Kimura, Keizo; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 561 - 568
反应条件
lithium in tetrahydrofuran
T=-30°C; 0.25 h;
参考文献
Guijarro, David; Mancheno, Balbino; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 28 p. 8551 - 8558
反应条件
methylcalcium iodide in tetrahydrofuran
T=-70°C; 3 h;
参考文献
Kanda, Takahiro; Sugino, Takushi; Kambe, Nobuaki; Sonoda, Noboru
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 67, # 1-4 p. 103 - 106
反应条件
cerium; iodine in tetrahydrofuran
T=25°C; 1 h;
参考文献
Fukuzawa, Shin-ichi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of Organometallic Chemistry, 1986 , vol. 299, p. 179 - 186
反应条件
1: 3-iodoprop-1-ene With chromium dichloride; H2Salen; triethylamine in acetonitrile
T=20°C; Metallation;
2: benzaldehyde With chloro-trimethyl-silane in acetonitrile
Addition;
参考文献
Bandini, Marco; Cozzi, Pier Giorgio; Melchiorre, Paolo; Umani-Ronchi, Achille
Angewandte Chemie - International Edition, 1999 , vol. 38, # 22 p. 3357 - 3359
反应条件
phenanthrene; N(Et)4ClO4 in N,N-dimethyl-formamide
T=0°C; Electrochemical reaction;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Chemistry Letters, 2003 , vol. 32, # 8 p. 720 - 721
反应条件
phenanthrene; N(Et)4ClO4 in N,N-dimethyl-formamide
T=0°C; Electrochemical reaction;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Chemistry Letters, 2003 , vol. 32, # 8 p. 720 - 721
反应条件
1: benzaldehyde dimethyl acetal; benzaldehyde With (2,7-dimethyl-1,8-biphenylenedioxy)bis(dimethylaluminum) in dichloromethane
T=-78°C; 0.0833333 h;
2: allyltributylstannane in dichloromethane
T=-78°C; 3 h;
3: With hydrogenchloride in dichloromethane
参考文献
Ooi, Takashi; Takahashi, Makoto; Yamada, Masao; Tayama, Eiji; Omoto, Kiyoyuki; Maruoka, Keiji
Journal of the American Chemical Society, 2004 , vol. 126, # 4 p. 1150 - 1160