1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
Ambient temperature;
参考文献
Bonini, Bianca Flavia; Comes-Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Nanni, Cristiano; Ricci, Alfredo
Tetrahedron Letters, 1998 , vol. 39, # 37 p. 6737 - 6740
反应条件
1: trans vinyl bromide; (CH3)3Al With bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran; toluene
T=70°C; Addition; 10 h;
2: benzaldehyde in tetrahydrofuran
Addition; 3 h;
参考文献
Hanzawa, Yuji; Kowase, Noboru; Momose, Shu-Ichi; Taguchi, Takeo
Tetrahedron, 1998 , vol. 54, # 38 p. 11387 - 11398
反应条件
tin(IV) chloride in dichloromethane
T=-78°C; Alkylation; Fragmentation;
参考文献
Dussault, Patrick H.; Lee, Hyung-Jae; Liu, Xuejun
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 17 p. 3006 - 3013
反应条件
silver(I) acetate in toluene
T=100°C; 15 h; Product distribution; Further Variations:ReagentsTemperaturesSolvents;
参考文献
Itami, Kenichiro; Kamei, Toshiyuki; Mineno, Masahiro; Yoshida, Jun-Ichi
Chemistry Letters, 2002 , # 11 p. 1084 - 1085
反应条件
1: benzaldehyde dimethyl acetal; benzaldehyde With titanium tetrachloride in dichloromethane
T=-78°C; 0.0833333 h;
2: allyltributylstannane in dichloromethane
T=-78°C; 3 h;
3: With hydrogenchloride in dichloromethane
参考文献
Ooi, Takashi; Takahashi, Makoto; Yamada, Masao; Tayama, Eiji; Omoto, Kiyoyuki; Maruoka, Keiji
Journal of the American Chemical Society, 2004 , vol. 126, # 4 p. 1150 - 1160
反应条件
4 A molecular sieve; tin(ll) chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in dichloromethane
T=20°C;
参考文献
Roy, Ujjal Kanti; Roy, Sujit
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7177 - 7180
反应条件
(vinyl)2Cu(CN)Li2 in tetrahydrofuran
1) -40 deg C, 30 min., 2) -30 deg C, 1h, 3) -20 deg C, 30 min.;
参考文献
Lipshutz, Bruce H.; Wilhelm, Robert S.; Kozlowski, Joseph A.; Parker, David
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3928 - 3938
反应条件
antimony; lithium iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
15 h; Heating;
参考文献
Butsugan, Yasuo; Ito, Hirokazu; Araki, Shuki
Tetrahedron Letters, 1987 , vol. 28, # 32 p. 3707 - 3708
反应条件
in water
Ambient temperature;
参考文献
Chan, Tak Hang; Yang, Yang; Li, Chao Jun
Journal of Organic Chemistry, 1999 , vol. 64, # 12 p. 4452 - 4455
反应条件
diethylzinc in hexane; dichloromethane
Ambient temperature;
参考文献
Huang, Wen-Hua; Huang, Yao-Zeng; Dai, Li-Xin
Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6953 - 6956
