1-苯基-3-丁烯-1-醇合成路线 (共 285 条)
反应条件
1: 82 percent / lithium aluminum hydride / diethyl ether / 6 h / Heating
2: 54 percent / pyridine / 36 h / Ambient temperature
3: acetonitrile; H2O / 20 h / Irradiation
View Scheme
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
potassium nitrate; tin(ll) chloride in water
T=25°C; 4 h; Electrochemical reaction;
参考文献
Zhang, Li; Zha, Zhenggen; Zhang, Zhenlei; Li, Yunfeng; Wang, Zhiyong
Chemical Communications, 2010 , vol. 46, # 38 p. 7196 - 7198
反应条件
tetrakis(triphenylphosphine) palladium(0); diethylzinc in tetrahydrofuran; hexane
5 h; Ambient temperature;
参考文献
Yasui, Kengo; Goto, Youichi; Yajima, Takafumi; Taniseki, Yasue; Fugami, Keigo; Tanaka, Akihiro; Tamaru, Yoshinao
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7619 - 7622
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol
12 h; Ambient temperature; Yield given;
参考文献
Angelaud, Remy
Tetrahedron Letters, 1995 , vol. 36, # 22 p. 3861 - 3864
反应条件
lt;V2Cl3(THF)6gt;2lt;Zn2Cl6gt; in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 0.5 h;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Tani, Kazuhide
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7083 - 7086
反应条件
4 A molecular sieve in toluene
40 h; Ambient temperature;
参考文献
Zhang, Luo Cheng; Sakurai, Hideki; Kira, Mitsuo
Chemistry Letters, 1997 , # 2 p. 129 - 130
反应条件
bis-(trifluoromethylsulphonyl)amine in dichloromethane
T=20°C; Sakurai-Hosomi allylation; 0.5 h; Product distribution;
参考文献
Ishihara; Hiraiwa; Yamamoto
Synlett, 2001 , # 12 p. 1851 - 1854
反应条件
ONOO(-); NADPH
T=10°C; 0.5 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Sheng, Xin; Zhang, Haoming; Im, Sang-Choul; Horner, John H.; Waskell, Lucy; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 2971 - 2976
反应条件
tetrakis(triphenylphosphine) palladium(0); diethylzinc in tetrahydrofuran; hexane
6 h; Ambient temperature;
参考文献
Yasui, Kengo; Goto, Youichi; Yajima, Takafumi; Taniseki, Yasue; Fugami, Keigo; Tanaka, Akihiro; Tamaru, Yoshinao
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7619 - 7622
反应条件
vanadium(III) chloride; benzaldehyde in diethyl ether; dichloromethane
14 h; -70 to 20 deg C in 14 h;
参考文献
Kauffmann, Thomas; Bonrath, Werner; Beirich, Christoph; Li, Weichang; Pahde, Claudia; et al.
Chemische Berichte, 1993 , vol. 126, # 9 p. 2093 - 2100