1-苯基-3-丁烯-1-醇合成路线 (共 285 条)
反应条件
cytochrome P 450 2B1; cytochrome reductase; NADPH; 1,2-dilauroylphosphatidylcholine in phosphate buffer
T=0 - 10°C; pH=7.4; 1 h; Kinetics; Further Variations:Reagents;
参考文献
Newcomb, Martin; Aebisher, David; Shen, Runnan; Chandrasena, R. Esala P.; Hollenberg, Paul F.; Coon, Minor J.
Journal of the American Chemical Society, 2003 , vol. 125, # 20 p. 6064 - 6065
反应条件
phenanthrene; N(Et)4ClO4; magnesium in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Tetrahedron, 2004 , vol. 60, # 8 p. 1791 - 1801
反应条件
phenanthrene; N(Et)4ClO4; magnesium in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Tetrahedron, 2004 , vol. 60, # 8 p. 1791 - 1801
反应条件
1: With chromium dichloride in tetrahydrofuran
T=20°C; Nozaki-Himaya reaction; 4 h;
2: With (1R,8S,9R)-bipyridyl derivative in tetrahydrofuran
T=20 - 55°C;
参考文献
Schrekker, Henri S.; Micskei, Karoly; Hajdu, Csongor; Patonay, Tamas; De Bolster, Martin W. G.; Wessjohann, Ludger A.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 7 p. 731 - 736
反应条件
[Rh(TMEDA)(CO2)][Rh(Cl)2(CO)2]; carbon monoxide; cesium carbonate hydrate; water-d2 in tetrahydrofuran
T=100°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Vasylyev, Maksym; Alper, Howard
Journal of Organic Chemistry, 2010 , vol. 75, # 8 p. 2710 - 2713
反应条件
Pd(CHCN)2Cl2; tin(ll) chloride in tetrahydrofuran
参考文献
Volla, Chandra M. R.; Markovic, Dean; Laclef, Sylvain; Vogel, Pierre
Chemistry - A European Journal, 2010 , vol. 16, # 30 p. 8984 - 8988
反应条件
1: benzyl alcohol With anhydrous iron chloride; indium; chloramine-T in dichloromethane
T=20°C; Inert atmosphere;
2: allyl bromide With indium in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Srivastava, Vishnu P.; Patel, Rajesh; Yadav, Lal Dhar S.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 695 - 700
反应条件
1: benzyl alcohol With anhydrous iron chloride; chloramine-T in tetrahydrofuran; water
T=20°C; Inert atmosphere;
2: allyl bromide With indium in tetrahydrofuran; water
T=20°C; Inert atmosphere;
参考文献
Srivastava, Vishnu P.; Patel, Rajesh; Yadav, Lal Dhar S.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 695 - 700
反应条件
tin(IV) chloride; tetra-(n-butyl)ammonium iodide in dichloromethane
T=20°C; 24 h;
参考文献
Masuyama, Yoshiro; Suga, Takanori; Watabe, Akiko; Kurusu, Yasuhiko
Tetrahedron Letters, 2003 , vol. 44, # 14 p. 2845 - 2847
反应条件
indium in water
16 h; Ambient temperature;
参考文献
Chen, Dong-Li; Li, Chao-Jun
Tetrahedron Letters, 1996 , vol. 37, # 3 p. 295 - 298