1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=0°C; 1 h;
参考文献
Asao, Naoki; Shibato, Atsushi; Itagaki, Yoshifumi; Jourdan, Fabrice; Maruoka, Keiji
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3177 - 3180
反应条件
cerium(III) chloride; zinc in tetrahydrofuran; benzene
T=43°C; Alkylation; destannylation; 2 h; ultrasound;
参考文献
Lee, Adam Shih-Yuan; Wu, Chen-Wen
Tetrahedron, 1999 , vol. 55, # 43 p. 12531 - 12542
反应条件
1: With (TfNHCH2)3CCH3*Me3Al in dichloromethane
T=20°C; 1.5 h;
2: Acid hydrolysis;
参考文献
Kanai, Motomu; Kuramochi, Akiyoshi; Shibasaki, Masakastu
Synthesis, 2002 , # 14 p. 1956 - 1958
反应条件
strontium in tetrahydrofuran
T=-20°C; Barbier reaction;
参考文献
Miyoshi, Norikazu; Kamiura, Koji; Oka, Hiromi; Kita, Akiko; Kuwata, Rika; Ikehara, Daitetsu; Wada, Makoto
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 2 p. 341 - 345
反应条件
methyltrioxorhenium (VII) in acetonitrile
T=20°C; 1 h;
参考文献
Pramanik, Suman; Ghorai, Prasanta
Chemical Communications, 2012 , vol. 48, # 12 p. 1820 - 1822
反应条件
4 A molecular sieve in toluene
40 h; Ambient temperature;
参考文献
Zhang, Luo Cheng; Sakurai, Hideki; Kira, Mitsuo
Chemistry Letters, 1997 , # 2 p. 129 - 130
反应条件
in dichloromethane
Ambient temperature;
参考文献
Chan, Tak Hang; Yang, Yang
Tetrahedron Letters, 1999 , vol. 40, # 20 p. 3863 - 3866
反应条件
1: n-BuLi
2: aq. TsOH / tetrahydrofuran; propan-2-ol
3: 96 percent / toluene / 14 h / 110 °C
4: 79 percent / TBAF / tetrahydrofuran
View Scheme
参考文献
Bashiardes, George; Chaussebourg, Vanessa; Laverdan, Geraldine; Pornet, Jacques
Chemical Communications, 2004 , # 1 p. 122 - 123
反应条件
1: 96 percent / toluene / 14 h / 110 °C
2: 79 percent / TBAF / tetrahydrofuran
View Scheme
参考文献
Bashiardes, George; Chaussebourg, Vanessa; Laverdan, Geraldine; Pornet, Jacques
Chemical Communications, 2004 , # 1 p. 122 - 123
反应条件
1: zirconocene dichloride; sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; dichloromethane; toluene / -20 - 20 °C / Inert atmosphere
2: tetrahydrofuran; dichloromethane; toluene / Inert atmosphere
View Scheme
参考文献
Oda, Yukiko; Sato, Takaaki; Chida, Noritaka
Organic Letters, 2012 , vol. 14, # 3 p. 950 - 953
