1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
1.1: BuLi / tetrahydrofuran / 0.5 h / -20 °C
1.2: 75 percent / tetrahydrofuran / 5 h / 20 °C
View Scheme
参考文献
Okuma, Kentaro; Kamahori, Yoshihiro; Tsubakihara, Kimiko; Yoshihara, Kanami; Tanaka, Yuichiro; Shioji, Kosei
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7355 - 7360
反应条件
1: pyridine / 36 h / Ambient temperature
2: acetonitrile; H2O / 20 h / Irradiation
View Scheme
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
1: 54 percent / pyridine / 36 h / Ambient temperature
2: acetonitrile; H2O / 20 h / Irradiation
View Scheme
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
in water; acetonitrile
20 h; Irradiation;
参考文献
Hixson; Franke; Gere; Xing
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3601 - 3610
反应条件
indium in N,N-dimethyl acetamide
T=0°C; 2 h; Yields of byproduct given;
参考文献
Hirashita, Tsunehisa; Kamei, Toshiya; Horie, Tomoaki; Yamamura, Hatsuo; Kawai, Masao; Araki, Shuki
Journal of Organic Chemistry, 1999 , vol. 64, # 1 p. 172 - 177
反应条件
n-BuMnMgBr
Addition;
参考文献
Nishikawa, Toshihiro; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron, 2003 , vol. 59, # 48 p. 9661 - 9668
反应条件
tin(IV) chloride in dichloromethane
T=-78°C; Alkylation; Fragmentation;
参考文献
Dussault, Patrick H.; Lee, Hyung-Jae; Liu, Xuejun
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 17 p. 3006 - 3013
反应条件
tin(IV) chloride in dichloromethane
T=-78°C; Alkylation; Fragmentation; Further byproducts given;
参考文献
Dussault, Patrick H.; Lee, Hyung-Jae; Liu, Xuejun
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 17 p. 3006 - 3013
反应条件
palladium diacetate; triphenylphosphine in dimethyl sulfoxide
T=100°C; 20 h;
参考文献
Kiji, Jitsuo; Okano, Tamon; Nomura, Takaaki; Saiki, Kayoko; Sai, Torei; Tsuji, Jiro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1939 - 1945
反应条件
4-nitro-benzoic acid in acetonitrile
T=20°C; 5 h;
参考文献
Li, Gui-Long; Zhao, Gang
Synthesis, 2006 , # 19 p. 3189 - 3194
