1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
titanium(IV) isopropylate in isopropyl alcohol
Meerwein-Ponndorf-Verley-Oppenauer reaction; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
Liu, Guohua; Gao, Yan; Lu, Xiaoquan; Liu, Mouming; Zhang, Fang; Li, Hexing
Chemical Communications, 2008 , # 27 p. 3184 - 3186
反应条件
1.) CuCN
2.) -10 deg C, 2.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lipshutz, Bruce H.; Kozlowski, Joseph; Wilhelm, Robert S.
Journal of the American Chemical Society, 1982 , vol. 104, # 8 p. 2305 - 2307
反应条件
tetrakis(triphenylphosphine) palladium(0); diethylzinc in tetrahydrofuran; hexane
6 h; Ambient temperature;
参考文献
Yasui, Kengo; Goto, Youichi; Yajima, Takafumi; Taniseki, Yasue; Fugami, Keigo; Tanaka, Akihiro; Tamaru, Yoshinao
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7619 - 7622
反应条件
zinc in tetrahydrofuran; ammonia
0.5 h;
参考文献
Makosza, Mieczyslaw; Grela, Karol
Synthetic Communications, 1996 , vol. 26, # 15 p. 2935 - 2940
反应条件
indium in N,N-dimethyl-formamide
T=0°C; 3 h;
参考文献
Araki, Shuki; Hirashita, Tsunebisa; Shimizu, Hidetaka; Yamamura, Hatsuo; Kawai, Masao; Butsugan, Yasuo
Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8417 - 8420
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane
168 h; Ambient temperature;
参考文献
Akiyama, Takahiko; Iwai, Junko
Synlett, 1998 , # 3 p. 273 - 274
反应条件
1: allyltributylstannane; (η3-allylPdCl)2 in tetrahydrofuran
T=-60 - -40°C; 1 h;
2: benzaldehyde; α-cyanoacetic acid methyl ester With triphenylphosphine in tetrahydrofuran
T=-40 - 20°C; Title compound not separated from byproducts;
参考文献
Kiji, Jitsuo; Okano, Tamon; Nomura, Takaaki; Saiki, Kayoko; Sai, Torei; Tsuji, Jiro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1939 - 1945
反应条件
catalyst: Pd(OAc)2-triphenylphosphine in tetrahydrofuran
under Ar; THF, CH2CHCH2Cl, allylstannane, NCCH2CO2CH3 and PhCHO added tomixt. of Pd(OAc)2 and PPh3 (molar ratio 17:19:11:10:1:2); heated at ref lux for 20 h; treated with water; extd. with ether; distd. under reduced pressure; detd. by GC;
参考文献
Kiji, Jitsuo; Okano, Tamon; Nomura, Takaaki; Saiki, Kayoko; Sai, Torei; Tsuji, Jiro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1939 - 1945
反应条件
malonic acid in diethyl ether
参考文献
Koenig,K.; Neumann,W.P.
Tetrahedron Letters, 1967 , p. 495 - 498
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane; water
0.75 h; Ambient temperatureeffect of the amount of Sc(OTf)3 and water and the reaction time; Product distribution;
参考文献
Akiyama, Takahiko; Iwai, Junko
Tetrahedron Letters, 1997 , vol. 38, # 5 p. 853 - 856
