1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
in diethyl ether
Addition; Product distribution;
参考文献
Holm, Torkil
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1188 - 1192
反应条件
sodium hydrogencarbonate
0.5 h; Heating; Product distribution;
参考文献
Chandrasena, R. Esala P.; Aebisher, David; Newcomb, Martin
Journal of Physical Organic Chemistry, 2005 , vol. 18, # 9 p. 974 - 977
反应条件
sodium hydrogencarbonate
0.5 h; Heating; Product distribution;
参考文献
Chandrasena, R. Esala P.; Aebisher, David; Newcomb, Martin
Journal of Physical Organic Chemistry, 2005 , vol. 18, # 9 p. 974 - 977
反应条件
RhH(CO)(triphenylphosphine)3; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran; water
T=130°C; P=6203.12 Torr; 0.666667 h; Microwave irradiation;
参考文献
Airiau, Etienne; Chemin, Claire; Girard, Nicolas; Lonzi, Giacomo; Mann, Andre; Petricci, Elena; Salvadori, Jessica; Taddei, Maurizio
Synthesis, 2010 , # 17 art. no. C03410SS, p. 2901 - 2914
反应条件
1: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 °C
2: potassium hydroxide / methanol / 20 °C
3: m-chloroperbenzoic acid / CH2Cl2 / 0 °C
4: 98 percent / (Cy3P)2(Cl)2Ru(=CHPh) / CH2Cl2 / 3.5 h / Heating
5: 78 percent / Br2CF2; KOH/Al2O3 / 2-methyl-propan-2-ol; tetrahydrofuran
View Scheme
参考文献
Yao, Qingwei
Organic letters, 2002 , vol. 4, # 3 p. 427 - 430
反应条件
indium(III) chloride in dichloromethane
T=20°C; 3 h;
参考文献
Merisor, Elena; Conrad, Juergen; Malakar, Chandi C.; Beifuss, Uwe
Synlett, 2008 , # 6 p. 903 - 907
反应条件
(i) NaH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Cui, Yong-Mei; Huang, Qing-Qing; Xu, Jie; Chen, Ling-Ling; Li, Jing-Ya; Ye, Qi-Zhuang; Li, Jia; Nan, Fa-Jun
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 18 p. 4130 - 4135
反应条件
1: 1.) NaH, 2.) n-BuLi / 1.) DMF, room temp., overnight, 2.) THF, hexane, -78 deg C, 20 min
2: n-Bu3SnH, Et3B, AIBN / toluene / -20 °C / other temp., other solvent, various molar ratio
View Scheme
参考文献
Rawal; Singh; Dufour; Michoud
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7718 - 7727
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in benzene
T=20°C;
参考文献
Smith, Catherine M.; O'Doherty, George A.
Organic Letters, 2003 , vol. 5, # 11 p. 1959 - 1962
反应条件
1: 91 percent / Zn; CuCl / diethyl ether / 16 h / 35 °C
2: 76 percent / Na2Cr2O7; conc. H2SO4 / diethyl ether; H2O / 5 h / 23 °C
View Scheme
参考文献
Bloodworth, A. J.; Korkodilos, Despoina
Tetrahedron Letters, 1991 , vol. 32, # 47 p. 6953 - 6956
