1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; ethylene,methyl acetate; carbon monoxide
参考文献
Kondo, Teruyuki; Kodoi, Kouichi; Nishinaga, Eiji; Okada, Takumi; Morisaki, Yasuhiro; Watanabe, Yoshihisa; Mitsudo, Take-Aki
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5587 - 5588
反应条件
triethylamine; palladium on activated charcoal in toluene T=200°C; 12 h;
参考文献
Coquerel, Yoann; Bremond, Paul; Rodriguez, Jean
Journal of Organometallic Chemistry, 2007 , vol. 692, # 22 p. 4805 - 4808
反应条件
1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.33 h / 20 °C 2: bis(1,1-diphenylphosphino)methane; tetracarbonylbis(μ-chloro)dirhodium(I) / ethylene glycol dimethyl ether / 20 h / 65 °C / |Inert atmosphere View Scheme
参考文献
Zhuo, Lian-Gang; Yao, Zhong-Ke; Yu, Zhi-Xiang
Organic Letters, 2013 , vol. 15, # 18 p. 4634 - 4637
反应条件
2: base 3: O3 / CH2Cl2 / -78 °C 4: NaBH4 / methanol View Scheme
参考文献
Master, Hosang E.; Newadkar; Rane; Kumar, Ashok
Tetrahedron Letters, 1996 , vol. 37, # 51 p. 9253 - 9254
反应条件
sodium hydrogen sulphate; hydroquinone T=120°C; P=30 Torr;
参考文献
Journal of the American Chemical Society, , vol. 128, # 26 p. 8559 - 8568
反应条件
2,4,6-trichloro-1,3,5-triazine in dichloromethane; N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Synthetic Communications, , vol. 37, # 24 p. 4367 - 4370
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / Heating 1.2: 90 percent / tetrahydrofuran / Heating 2.1: 90 percent / [Cl2(PCy3)2Ru=CHPh] / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 22 p. 7672 - 7687
反应条件
palladium dichloride T=50°C; 3 h; under air;
参考文献
Tan, Jiajing; Zhang, Zuhui; Wang, Zhiyong
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 8 p. 1344 - 1348
反应条件
1: 92 percent / Et3N / CH2Cl2 / 2 h / 20 °C 2: 95 percent / [(CF3)2C(Me)O]2Mo[CHCMe2Ph][N-(2,6-diisopropylphenyl)] / benzene / 1 h / 20 °C View Scheme
参考文献
Denmark, Scott E.; Yang, Shyh-Ming
Organic Letters, 2001 , vol. 3, # 11 p. 1749 - 1752
反应条件
1: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 °C 2: potassium hydroxide / methanol / 20 °C 3: m-chloroperbenzoic acid / CH2Cl2 / 0 °C 4: 100 percent / (Cy3P)2(Cl)2Ru(=CHPh) / CH2Cl2 / 2 h / Heating View Scheme
参考文献
Yao, Qingwei
Organic letters, 2002 , vol. 4, # 3 p. 427 - 430
