1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
InI; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; allylation; 1.5 h;
参考文献
Araki, Shuki; Kamei, Toshiya; Hirashita, Tsunehisa; Yamamura, Hatsuo; Kawai, Masao
Organic Letters, 2000 , vol. 2, # 6 p. 847 - 849
反应条件
InI; triphenylphosphine; bis(acetylacetonate)nickel(II) in various solvent(s)
T=20°C; 24 h;
参考文献
Hirashita, Tsunehisa; Kambe, Shinya; Tsuji, Hiromitsu; Omori, Hideki; Araki, Shuki
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5054 - 5059
反应条件
1: With N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran
T=-20°C; 5 h; Inert atmosphereSealed flask;
2: With water; ammonium chloride in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Lewis, Frank W.; McCabe, Thomas C.; Grayson, David H.
Tetrahedron, 2011 , vol. 67, # 39 p. 7517 - 7528
反应条件
1: With indium in N,N-dimethyl acetamide
T=20°C; 1 h;
2: With iodobenzene; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl acetamide
T=20°C; 24 h; Further stages.;
参考文献
Hirashita; Yamamura; Kawai; Araki
Chemical Communications, 2001 , # 4 p. 387 - 388
反应条件
1: α,α-diisopropylhomoallylic alcohol With methyl-magnesium iodide in 1,4-dioxane
T=25°C; 1 h;
2: benzaldehyde With gallium(III) chloride in 1,4-dioxane; hexane
T=25°C; 13 h;
参考文献
Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of Organometallic Chemistry, 2007 , vol. 692, # 1-3 p. 505 - 513
反应条件
tin(ll) chloride; bis(benzonitrile)palladium(II) dichloride in tetrahydrofuran; water
T=50°C; 24 h;
参考文献
Masuyama, Yoshiro; Marukawa, Masanori
Tetrahedron Letters, 2007 , vol. 48, # 34 p. 5963 - 5965
反应条件
1: benzaldehyde With ammonia in ethanol
T=-10°C; 2 h;
2: allylboronic acid pinacol ester in ethanol
T=-10 - 20°C; 4 h;
参考文献
Sugiura, Masaharu; Hirano, Keiichi; Kobayashi, Shu
Journal of the American Chemical Society, 2004 , vol. 126, # 23 p. 7182 - 7183
反应条件
zirconocene dichloride; ethylmagnesium bromide in tetrahydrofuran
T=-78 - 20°C;
参考文献
Barluenga, Jose; Alvarez-Rodrigo, Lucia; Rodriguez, Felix; Fananas, Francisco J.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 38 p. 6362 - 6365
反应条件
in tetrahydrofuran; diethyl ether
T=20°C; 3.5 h; Inert atmosphere;
参考文献
Hudrlik, Paul F.; Hudrlik, Anne M.; Jeilani, Yassin A.
Tetrahedron, 2011 , vol. 67, # 52 p. 10089 - 10096
反应条件
indium(III) chloride; indium; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water
T=20°C; 5 h;
参考文献
Jang, Taeg-Su; Keum, Gyochang; Kang, Soon Bang; Chung, Bong Young; Kim, Youseung
Synthesis, 2003 , # 5 p. 775 - 779
