1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
diethylzinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
2 h; Heating;
参考文献
Clayden, Jonathan; Julia, Marc
Journal of the Chemical Society, Chemical Communications, 1994 , # 16 p. 1905 - 1906
反应条件
InI; triphenylphosphine; bis(acetylacetonate)nickel(II) in various solvent(s)
T=20°C; 1 h;
参考文献
Hirashita, Tsunehisa; Kambe, Shinya; Tsuji, Hiromitsu; Omori, Hideki; Araki, Shuki
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5054 - 5059
反应条件
bromo-dimethylsulfonium bromide in methanol
T=20°C; 6 h;
参考文献
Rani, Shikha; Babu, J. Lokesh; Vankar, Yashwant D.
Synthetic Communications, 2003 , vol. 33, # 23 p. 4043 - 4052
反应条件
1: C13H19BrOSi in diethyl ether
T=20°C; 1.5 h; Inert atmosphere;
2: benzaldehyde in tetrahydrofuran; diethyl ether
T=20°C; 8 h;
参考文献
Hudrlik, Paul F.; Hudrlik, Anne M.; Jeilani, Yassin A.
Tetrahedron, 2011 , vol. 67, # 52 p. 10089 - 10096
反应条件
bismuth(III) chloride; iron in tetrahydrofuran
4.5 h; Ambient temperature;
参考文献
Wada, Makoto; Ohki, Hidenori; Akiba, Kin-ya
Tetrahedron Letters, 1986 , vol. 27, # 39 p. 4771 - 4774
反应条件
benzene-1,2-diol; triethylamine
T=50°C; 12 h; variation of aldehydes, variation of hydroxy compounds, variation of amines;
参考文献
Aoyama, Naohiro; Hamada, Tomoaki; Manabe, Kei; Kobayashi, Shu
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7329 - 7333
反应条件
in diethyl ether
T=0°C; 1.5 h; Inert atmosphere;
参考文献
Stefan, Eric; Nalin, Ansel P.; Taylor, Richard E.
Tetrahedron, 2013 , vol. 69, # 36 p. 7706 - 7712
反应条件
InI; triphenylphosphine; bis(acetylacetonate)nickel(II) in tetrahydrofuran
T=20°C; 5 h;
参考文献
Hirashita, Tsunehisa; Kambe, Shinya; Tsuji, Hiromitsu; Omori, Hideki; Araki, Shuki
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5054 - 5059
反应条件
1: With Me2AlNTf2 in dichloromethane
T=-20°C; Addition; 3 h;
2: With hydrogenchloride; water in tetrahydrofuran; dichloromethane
T=20°C; Hydrolysis; 0.5 h;
参考文献
Marx, Andreas; Yamamoto, Hisashi
Angewandte Chemie - International Edition, 2000 , vol. 39, # 1 p. 178 - 181
反应条件
indium monobromide; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; palladium diacetate
0.4 h;
参考文献
Fontana, Gianfranco; Lubineau, Andre; Scherrmann, Marie-Christine
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1375 - 1380
