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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
80776-33-6
合成路线
（共 11 条）
80776-30-3
→
反应条件
80776-33-6
反应条件
hydrogenchloride; soude a 4 h; Heating1) ethanol, 2) eau;
参考文献
Lancelot, Jean-Charles; Gazengel, Jean-Marie; Robba, Max
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1281 - 1285
6954-68-3
→
反应条件
80776-33-6
反应条件
1: 67 percent / acide nitrique fumant / acetic acid / 1.5 h / 30 °C 2: 50 percent / acide nitrique fumant / acetic acid / 2.5 h / 45 °C 3: 83 percent / 1) acide chlorhydrique, 2) soude a 20percent / 4 h / Heating; 1) ethanol, 2) eau View Scheme
参考文献
Lancelot, Jean-Charles; Gazengel, Jean-Marie; Robba, Max
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1281 - 1285
80776-24-5
→
反应条件
80776-33-6
反应条件
1: 50 percent / acide nitrique fumant / acetic acid / 2.5 h / 45 °C 2: 83 percent / 1) acide chlorhydrique, 2) soude a 20percent / 4 h / Heating; 1) ethanol, 2) eau View Scheme
参考文献
Lancelot, Jean-Charles; Gazengel, Jean-Marie; Robba, Max
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1281 - 1285
64-18-6
甲酸
+
80776-33-6
→
反应条件
80776-31-4
反应条件
1.5 h; Heating;
参考文献
Lancelot, Jean-Charles; Gazengel, Jean-Marie; Robba, Max
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1281 - 1285
696-59-3
2,5-二甲氧基四氢呋喃
+
80776-33-6
→
反应条件
82982-96-5
反应条件
in acetic acid 1.5 h; Heating;
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
80776-33-6
→
反应条件
82982-97-6
反应条件
1: 81 percent / acetic acid / 1.5 h / Heating 2: 90 percent / hydrogen / Raney nickel / ethanol / 1.5 h / 110 °C / 73550.8 Torr View Scheme
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
80776-33-6
→
反应条件
82983-06-0
反应条件
1: 81 percent / acetic acid / 1.5 h / Heating 2: 90 percent / hydrogen / Raney nickel / ethanol / 1.5 h / 110 °C / 73550.8 Torr 3: 67 percent / toluene / 1 h / Heating View Scheme
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
80776-33-6
→
反应条件
82983-07-1
反应条件
1: 81 percent / acetic acid / 1.5 h / Heating 2: 90 percent / hydrogen / Raney nickel / ethanol / 1.5 h / 110 °C / 73550.8 Torr 3: 67 percent / toluene / 1 h / Heating 4: 42 percent / 3 h / Heating 5: 50 percent / 40percent sodium hydroxide / 3 h / Heating View Scheme
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
80776-33-6
→
反应条件
82983-11-7
反应条件
1: 81 percent / acetic acid / 1.5 h / Heating 2: 90 percent / hydrogen / Raney nickel / ethanol / 1.5 h / 110 °C / 73550.8 Torr 3: 67 percent / toluene / 1 h / Heating 4: 51 percent / 3 h / Heating View Scheme
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
80776-33-6
→
反应条件
82983-12-8
反应条件
1: 81 percent / acetic acid / 1.5 h / Heating 2: 90 percent / hydrogen / Raney nickel / ethanol / 1.5 h / 110 °C / 73550.8 Torr 3: 67 percent / toluene / 1 h / Heating 4: 40 percent / 3 h / Heating View Scheme
参考文献
Lancelot; Gazengel; Rault; Robba
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1674 - 1679
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