1H,1H,1H-全氟-2-辛酮合成路线 （共 13 条）
反应条件
potassium fluoride in various solvent(s)
T=120°C; P=200 Torr;
参考文献
Hedhli, A.; Chaabouni, M. M.; Baklouti, A.
Journal of Fluorine Chemistry, 1992 , vol. 56, # 2 p. 239 - 247
反应条件
sulfuric acid; mercuric sulphate in methanol; water
T=70°C; 7 h;
参考文献
Moreau,P.; Naji,N.
Journal of Fluorine Chemistry, 1987 , vol. 34, p. 421
反应条件
in diethyl ether
T=-45°C; 5 h;
参考文献
Batizat, D. V.; Yarosh, A. A.; Ignatenko, A. V.; Ponomarenko, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 5 p. 1022 - 1024
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1163 - 1165
反应条件
in diethyl ether
T=-40°C; 5 h;
参考文献
Batizat, D. V.; Yarosh, A. A.; Ignatenko, A. V.; Ponomarenko, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 5 p. 1022 - 1024
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1163 - 1165
反应条件
2,2'-azo-bisisobutyronitrile; copper; zinc
0.333333 h; Ambient temperature;
参考文献
Benefice-Malouet, S.; Commeyras, A.
Journal of Fluorine Chemistry, 1995 , vol. 70, # 1 p. 103 - 108
反应条件
in diethyl ether
2 h; Heating;
参考文献
Croxtal, Ben; Fawcett, John; Hope, Eric G.
Journal of Fluorine Chemistry, 2003 , vol. 119, # 1 p. 65 - 73
反应条件
1: 90 percent / pyridine / diethyl ether / 1 h / 0 °C
2: 95 percent / KF / various solvent(s) / 120 °C / 200 Torr
View Scheme
参考文献
Hedhli, A.; Chaabouni, M. M.; Baklouti, A.
Journal of Fluorine Chemistry, 1992 , vol. 56, # 2 p. 239 - 247
反应条件
in diethyl ether
T=-20°C;
参考文献
Wrackmeyer, Bernd; Werner, Konrad Von; Wehowsky, Frank
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 359 - 372
反应条件
in diethyl ether
T=-70°C; 6 h;
参考文献
Batizat, D. V.; Yarosh, A. A.; Ignatenko, A. V.; Ponomarenko, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 5 p. 1022 - 1024
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1163 - 1165
反应条件
in diethyl ether
T=-30°C; 2 h; other temperature, time; Product distribution;
参考文献
Batizat, D. V.; Yarosh, A. A.; Ignatenko, A. V.; Ponomarenko, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 5 p. 1022 - 1024
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1163 - 1165
