5,6-二氢-2-甲基-5-氧代-1,6-萘啶-3-羧酸乙酯合成路线 (共 4 条)
反应条件
sodium ethanolate in ethanol
2 h; Heating;
参考文献
Balogh; Hermecz; Simon; Pusztay
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 6 p. 1755 - 1769
反应条件
ammonium hydroxide in ethanol
36 h; Ambient temperature;
参考文献
Balogh, Maria; Hermecz, Istvan; Naray-Szabo, Gabor; Simon, Kalman; Meszaros, Zoltan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 753 - 758
反应条件
1: 98 percent / acetic acid / 0.5 h / 100 °C
2: 55.5 percent / NaOEt / ethanol / 2 h / Heating
View Scheme
参考文献
Balogh, Maria; Hermecz, Istvan; Naray-Szabo, Gabor; Simon, Kalman; Meszaros, Zoltan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 753 - 758
反应条件
1: 50.7 percent / 1.) 140 deg C, 6 h; 2.) 4 deg C, 2 d;
2: 64.3 percent / 25 percent aq. ammonium hydroxide / ethanol / 36 h / Ambient temperature
View Scheme
参考文献
Balogh, Maria; Hermecz, Istvan; Naray-Szabo, Gabor; Simon, Kalman; Meszaros, Zoltan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 753 - 758