反应条件
1: 100 percent / trimethylchlorosilane / 20 °C
2: 90 percent / 4-dimethylaminopyridine; triethylamine / CH2Cl2 / 1 h / 20 °C
3: BH3-DMS / tetrahydrofuran / -10 - 20 °C
4: 0.16 g / hydrochloric acid / ethanol; tetrahydrofuran / 1 h / Heating
5: 100 percent / Amberlite IRA 400 (OH(1-)); aqueous acetic acid
View Scheme
参考文献
Felluga, Fulvia; Gombac, Valentina; Pitacco, Giuliana; Valentin, Ennio
Tetrahedron Asymmetry, 2004 , vol. 15, # 20 p. 3323 - 3327
