3-(3-双吖丙啶基)苯酚合成路线 （共 3 条）
反应条件
hydrogenchloride in acetic acid
2 h;
参考文献
Leblanc; Gerber
Canadian Journal of Chemistry, 1984 , vol. 62, # 9 p. 1767 - 1771
反应条件
1: 1.) ammonia, tert-butyl hypochlorite, 2.) tert-butyl hypochlorite / 1.) methanol, tert-butyl alcohol, -40 deg C, 1 h; -40 deg C - room temperature, 2.) 0 deg C, 3 h
2: HCl / acetic acid
View Scheme
参考文献
Radhakrishnan, Ramachandran; Costello, Catherine E.; Khorana, H. Gobind
Journal of the American Chemical Society, 1982 , vol. 104, # 14 p. 3990 - 3997
反应条件
1: NaOCH3
2: 1.) ammonia, tert-butyl hypochlorite, 2.) tert-butyl hypochlorite / 1.) methanol, tert-butyl alcohol, -40 deg C, 1 h; -40 deg C - room temperature, 2.) 0 deg C, 3 h
3: HCl / acetic acid
View Scheme
参考文献
Radhakrishnan, Ramachandran; Costello, Catherine E.; Khorana, H. Gobind
Journal of the American Chemical Society, 1982 , vol. 104, # 14 p. 3990 - 3997
