3-甲氧基-4-硝基苯甲醇合成路线 （共 8 条）
反应条件
boric acid trimethyl ester; dimethylsulfide borane complex in tetrahydrofuran Reduction; 6 h; Heating;
参考文献
Hay, Michael P.; Sykes, Bridget M.; Denny, William A.; O'Connor, Charmian J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2759 - 2770
反应条件
aluminum isopropoxide; isopropyl alcohol
参考文献
Journal of the Chemical Society, , p. 221 - 222
反应条件
hydrazine hydrate; palladium on activated charcoal in methanol 1.75 h; Heating;
参考文献
Garcia, C.; Malthete, J.; Collet, A.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, # 1 p. 93 - 95
反应条件
carbon tetrabromide; triphenylphosphine in tetrahydrofuran T=20°C; 24 h; ConcentrationTime;
参考文献
CANCER RESEARCH TECHNOLOGY LIMITED; Bavetsias, Vassilios; Atrash, Butrus; Naud, Sébastien Gaston André; Sheldrake, Peter William; Blagg, Julian
Patent: US2013/345181 A1, 2013 ;
Location in patent: Paragraph 0713 ;
反应条件
triphenylphosphine in tetrahydrofuran T=20°C;
参考文献
CANCER RESEARCH TECHNOLOGY LIMITED; BAVETSIAS, Vassilios; ATRASH, Butrus; NAUD, Sebastien Gaston Andre; SHELDRAKE, Peter William; BLAGG, Julian
Patent: WO2012/123745 A1, 2012 ;
Location in patent: Page/Page column 87 ;
WO 2012/123745 A1
参考文献
Keegan, Kathleen S.; Kesicki, Edward A.; Gaudino, John Joseph; Cook, Adam Wade; Cowen, Scott Douglas; Burgess, Laurence Edward
Patent: US2003/69284 A1, 2003 ;
US 20030069284 A1
反应条件
thionyl chloride
12 h; Reflux;
参考文献
OSI PHARMACEUTICALS, LLC; CREW, Andrew, P.; DONG, Hanqing; FERRARO, Caterina; SHERMAN, Dan; SIU, Kam, W.
Patent: WO2012/74951 A1, 2012 ;
Location in patent: Page/Page column 36 ;
WO 2012/074951 A1
反应条件
dipyridinium dichromate in dichloromethane
T=23°C; Oxidation; 16 h;
参考文献
Pinney, Kevin G.; Mejia, Maria P.; Villalobos, Victor M.; Rosenquist, Brent E.; Pettit, George R.; Verdier-Pinard, Pascal; Hamel, Ernest
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 10 p. 2417 - 2425
