7-氧代胆甾-5-烯-3-beta-基乙酸酯合成路线 (共 77 条)
反应条件
1: 90 percent / Pb(OAc)4 / cyclohexane / 1 h / Ambient temperature 2: 89 percent / Al2O3 / benzene / Ambient temperature View Scheme
参考文献
Synthesis, , # 12 p. 1055 - 1058
反应条件
chromium(VI) oxide; acetic acid T=97°C;
参考文献
Journal of the Chemical Society, , p. 759
反应条件
chromium(VI) oxide; acetic acid T=25°C;
参考文献
Journal of the Chemical Society, , p. 1798,1800
反应条件
T=160°C; 1 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2325 - 2328
反应条件
pyridine; pyridine-2-carboxylic acid; dihydrogen peroxide; acetic anhydride; iron (III) perchlorate in acetonitrile 0.5 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 47, # 1 p. 64 - 70
反应条件
nitric acid; bentonite Irradiation;
参考文献
Jimenez-Estrada, Manuel; Garcia, M. Olivia; Navarro, Arturo O.; Eusebio, Jose L.; Alvarez, Cecilio T.; Penieres, Guillermo C.; Gutierrez, Rene P.
Steroids, 1997 , vol. 62, # 6 p. 500 - 503
反应条件
tris(acetylacetonato)iron in acetonitrile 24 h; Heatingvar. solv., reag; add of cat.;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 6 p. 1836 - 1841
反应条件
T=160°C; 1 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2325 - 2328
反应条件
ferric picolinate complexes; dihydrogen peroxide in acetonitrile 3 h; Ambient temperature; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 4 p. 750 - 752
反应条件
tris(acetylacetonato)iron in acetonitrile 24 h; Heatingvar. solv., reag; add of cat.;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 6 p. 1836 - 1841