3-(叔丁氧基羰基)丙基 4-甲基苯磺酸盐合成路线 (共 5 条)
反应条件
N-ethyl-N,N-diisopropylamine in chloroform Heating;
参考文献
Curran, Timothy P.; Pollastri, Michael P.; Abelleira, Susan M.; Messier, Renee J.; McCollum, Theresa A.; Rowe, Campbell G.
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5409 - 5412
反应条件
triethylamine in dichloromethane; water; ethyl acetate
参考文献
Tanabe Seiyaku Co., Ltd.
Patent: US5837673 A1, 1998 ;
反应条件
in pyridine; methanol; chloroform; water
参考文献
Zaidan Hojin Biseibutsu Kagaku Kenkyu Kai
Patent: US4518532 A1, 1985 ;
反应条件
in pyridine; methanol; chloroform; water
参考文献
Zaidan Hojin Biseibutsu Kagaku Kenkyu Kai
Patent: US4518802 A1, 1985 ;
反应条件
1.1: triethylamine / dichloromethane / 0.08 h / 20 °C / |Inert atmosphere
1.2: 10 h / 20 °C / |Inert atmosphere
2.1: triethylamine / dichloromethane / 2.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Zhang, Huan; Tanimoto, Hiroki; Morimoto, Tsumoru; Nishiyama, Yasuhiro; Kakiuchi, Kiyomi
Organic Letters, 2013 , vol. 15, # 20 p. 5222 - 5225