3-氨基-4-甲基-戊酸乙酯合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Birkofer; Erlenbach
Chemische Berichte, 1958 , vol. 91, p. 2383,2385
反应条件
1: 91 percent / H2 / PtO2 / acetic acid; ethyl acetate / 2 h / 760 Torr / Ambient temperature
2: 1.) 12N HCl; 2.) SOCl2 / 1.) acetic acid, 110 degC, 48h; 2.) 1h, room temp.; 6h, 40 degC
View Scheme
参考文献
Slopianka, Marion; Gossauer, Albert
Liebigs Annalen der Chemie, 1981 , # 12 p. 2258 - 2265
参考文献
Birkofer; Erlenbach
Chemische Berichte, 1958 , vol. 91, p. 2383,2385
反应条件
1: water; NH3
2: ethanolic HCl
View Scheme
参考文献
Birkofer; Erlenbach
Chemische Berichte, 1958 , vol. 91, p. 2383,2385
反应条件
hydrogenchloride; thionyl chloride
1.) acetic acid, 110 degC, 48h; 2.) 1h, room temp.; 6h, 40 degC; Yield given. Multistep reaction;
参考文献
Slopianka, Marion; Gossauer, Albert
Liebigs Annalen der Chemie, 1981 , # 12 p. 2258 - 2265
参考文献
Gedey, Szilvia; Liljeblad, Arto; Lazar, Laszlo; Fueloep, Ferenc; Kanerva, Liisa T.
Canadian Journal of Chemistry, 2002 , vol. 80, # 6 p. 565 - 570
