80937-33-3合成路线 (共 1249 条)
反应条件
in N,N-dimethyl-formamide
T=60°C; 48 h; Kinetics; TemperatureConcentration;
参考文献
Varadi, Tuende; Pap, Jozsef S.; Giorgi, Michel; Parkanyi, Laszlo; Csay, Tamas; Speier, Gabor; Kaizer, Jozsef
Inorganic Chemistry, 2013 , vol. 52, # 3 p. 1559 - 1569
反应条件
in neat (no solvent)
Electric Arc; O2 at ca. 3 atm expansion through pulsed molecular beam valve into reservoir with H2NCN and finally through pulsed electric discharge, accordingto T. R. Taylor et al., Chem. Phys. Lett. 301 (1999) 413; negative ions acceleration to 8 keV and sepn. temporally by Bakker TOF mass spectrometer;
参考文献
Bise, Ryan T.; Choi, Hyeon; Neumark, Daniel M.
Journal of Chemical Physics, 1999 , vol. 111, # 11 p. 4923 - 4932
反应条件
sodium hydroxide; 3-isopropyl-1-(2-hydroperoxy-2-propyl)benzene in water
T=90°C;
参考文献
Indspec Chemical Corporation
Patent: US6350921 B1, 2002 ;
Location in patent: Example 1 ;
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2, page 180 - 189
参考文献
Gmelin Handbook: B: B-Verb.13, 4.5.3.3, page 160 - 167
反应条件
in gas
byproducts: H2; with dry O2 at 40-80°C;;
参考文献
Gmelin Handbook: B: B-Verb.14, 4.4.2.5, page 192 - 192
反应条件
in gaseous matrix
Irradiation (UV/VIS); high-temperature alumina furnice (1240°C, 1E-7 bar), SiCl4/O2 ratio 1:1, Ar matrix (dilution 200:1), condensation on copper block (15 K, 30 min), irradiation (254 nm, 10 min), further product; IR-monitoring;
参考文献
Junker; Wilkening; Binnewies; Schnockel
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1531 - 1535
反应条件
decane
T=30°C; Inert atmosphere;
参考文献
Liu, Shujuan; Zheng, Zhen; Li, Minrui; Wang, Xinling
Research on Chemical Intermediates, 2012 , vol. 38, # 8 p. 1893 - 1907
反应条件
decane
T=30°C; Inert atmosphere;
参考文献
Liu, Shujuan; Zheng, Zhen; Li, Minrui; Wang, Xinling
Research on Chemical Intermediates, 2012 , vol. 38, # 8 p. 1893 - 1907
反应条件
3-methyl-pentane
T=30°C; Inert atmosphere;
参考文献
Liu, Shujuan; Zheng, Zhen; Li, Minrui; Wang, Xinling
Research on Chemical Intermediates, 2012 , vol. 38, # 8 p. 1893 - 1907