80937-33-3合成路线 （共 1249 条）
参考文献
Gmelin Handbook: S: MVol.B3, 100.101, page 1293 - 1530
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S: MVol.B3 (1963) pp. 1420-1433
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S: MVol.B3 (1963) pp. 1470-1511
反应条件
in acetonitrile
purging soln. of Ni-complex with SO2, then stirring under 1 atm O2 for 24 h (pptn.); filtration off of Ni-complex, detn. of SO4(2-) in filtrate by pptn. with BaCl2;
参考文献
Darensbourg, Marcetta Y.; Tuntulani, Thawatchai; Reibenspies, Joseph H.
Inorganic Chemistry, 1995 , vol. 34, p. 6287 - 6294
反应条件
in acetonitrile
purging soln. of Ni-complex with SO2, then stirring under 1 atm O2 for 24 h (pptn.); filtration off of Ni-complex, detn. of SO4(2-) in filtrate by pptn. with BaCl2;
参考文献
Darensbourg, Marcetta Y.; Tuntulani, Thawatchai; Reibenspies, Joseph H.
Inorganic Chemistry, 1995 , vol. 34, p. 6287 - 6294
反应条件
in neat (no solvent)
byproducts: CuO; roasting of briquetted CuS in air at 430 to 965°C, mechanism described;; formation of gaseous SO2 and solid CuO, at least formation of sulfate;;
参考文献
Peretti, E. A.
Discussions of the Faraday Society, 1948 , # 4 p. 174 - 179
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Gmelin Handbook: S: MVol.B1, 83, page 183 - 185
反应条件
in neat (no solvent)
byproducts: Cu-oxide; roasting of Cu-ore, react. described;;
参考文献
Ashcroft, E. A.
Trans. Electrochem. Soc., 1933 , vol. 63, p. 23 - 50
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Gmelin Handbook: S: MVol.B1, 83, page 183 - 185
反应条件
in water
using oxygen-saturated solns.; addn. of sulfite soln. to soln. of copper(II) tetraglycine (containing Ni(II) as impurity) at pH = 7 and 25°C; monitoring by UV;
参考文献
Moreno, Ruben G. M.; Alipazaga, Maria V.; Medeiros, Marisa H. G.; Coichev, Nina
Dalton Transactions, 2005 , # 6 p. 1101 - 1107
反应条件
in neat (no solvent)
Electric Arc; O2 at ca. 3 atm expansion through pulsed molecular beam valve into reservoir with H2NCN and finally through pulsed electric discharge, accordingto T. R. Taylor et al., Chem. Phys. Lett. 301 (1999) 413; negative ions acceleration to 8 keV and sepn. temporally by Bakker TOF mass spectrometer;
参考文献
Bise, Ryan T.; Choi, Hyeon; Neumark, Daniel M.
Journal of Chemical Physics, 1999 , vol. 111, # 11 p. 4923 - 4932
反应条件
in neat (no solvent)
100°C, 60 h; further products;
参考文献
Razuvaev, G. A.; Zhil'tsov, S. F.; Shabanov, A. V.; Lavrent'ev, A. A.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 454 - 462
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 567 - 575
反应条件
in neat (no solvent)
85°C, 15 h; further products;
参考文献
Razuvaev, G. A.; Zhil'tsov, S. F.; Shabanov, A. V.; Lavrent'ev, A. A.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 454 - 462
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 567 - 575
反应条件
in neat (no solvent)
150°C, 50 h; further products;
参考文献
Razuvaev, G. A.; Zhil'tsov, S. F.; Shabanov, A. V.; Lavrent'ev, A. A.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 454 - 462
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 567 - 575
