80937-33-3合成路线 (共 1249 条)
反应条件
Kinetics; Irradiation (UV/VIS); photochemical oxidn., ambient temp.;
参考文献
Marsh; Heicklen
Journal of Physical Chemistry, 1966 , vol. 70, p. 3008
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Gmelin Handbook: C: MVol.D3, 2.1.1.10, page 19 - 20
反应条件
catalyst: V2O5/TiO2 in neat (no solvent)
Kinetics; preheating of catalyst (V2O5 supported on TiO2) with O2 at 773 K for 2 h in quartz reactor; mixing of satd. o-dichlorobenzene/N2 stream with O2, preheating and introduction into reactor; heating up to 773 K; chromy.;
参考文献
Krishnamoorthy, Sundaram; Rivas, Juan A.; Amiridis, Michael D.
Journal of Catalysis, 2000 , vol. 193, # 2 p. 264 - 272
反应条件
in neat (no solvent)
explosion by electric spark;;
参考文献
Dixon; Harker
Mem. Pr. Manchester Soc. {4}, 1890 , vol. 3, p. 119 - 119
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Gmelin Handbook: Cl: MVol., 25, page 86 - 87
反应条件
metasilicic acid in melt
byproducts: oxides; formation of HCl as by-product;;
参考文献
Lichtenberger, T.; Kaiser, L.
Patent: DE470539 , 1929 ;
C. I, 1929 , p. 1726
反应条件
in neat (no solvent)
mixing NaCl with Cr2O3; heating the mixture with H2O vapor at red heat;;
参考文献
Kessler
Bulletin de la Societe Chimique de France, 1867 , vol. 8, p. 299 - 299
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Swindells
Jber. ch. Technol., 1851 , p. 695 - 695
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Gmelin Handbook: Na: MVol., 255, page 710 - 711
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Kessler
Patent: FR75305 , 1867 ;
反应条件
air; hydrogen in gas
TiCl4 (liq.) evapd.; oxidized in a diffusion flame reactor contg. 5 concentric tubes; reactor with multipoint diffusion-type burner; flame configuration Ar+TiCl4/Ar/H2/O2/air;
参考文献
Jang, Hee Dong; Kim, Seong-Kil
Materials Research Bulletin, 2001 , vol. 36, # 3-4 p. 627 - 637
反应条件
in gas
Irradiation (UV/VIS); on photolysis (>= 300nm, 1min irradiation) of a Cl2-SiHCl3-air-mixture (0.5 Torr Cl2, 1.0 Torr SiHCl3, 700 Torr air);; not isolated, monitoring of react. by IR (assignment proved by isotope labeling with (18)O2);;
参考文献
Niki, H.; Maker, P. D.; Savage, C. M.; Breitenbach, L. P.; Hurley, M. D.
Journal of Physical Chemistry, 1985 , vol. 89, # 17 p. 3725 - 3729
参考文献
Wang, Xiuyan; Suto, Masako; Lee, L. C.
Journal of Chemical Physics, 1988 , vol. 88, # 2 p. 896 - 899
反应条件
in gas
Irradiation (UV/VIS); on photolysis (>= 300nm, 1min irradiation) of a Cl2-SiHCl3-air-mixture (0.5 Torr Cl2, 1.0 Torr SiHCl3, 700 Torr air);; not isolated, monitoring of react. by IR;;
参考文献
Niki, H.; Maker, P. D.; Savage, C. M.; Breitenbach, L. P.; Hurley, M. D.
Journal of Physical Chemistry, 1985 , vol. 89, # 17 p. 3725 - 3729
反应条件
in neat (no solvent)
deflagration by electric spark;;
参考文献
Boetsch
Liebigs Annalen der Chemie, 1881 , vol. 210, p. 244 - 244
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Gmelin Handbook: Cl: MVol., 25, page 86 - 87