in neat (no solvent)
Kinetics; applying satd. aq. soln. of CaCl2 to Al2O3, evapn. of water, drying at 250°C to constant weight, kinetic study by gravimetric method, heating to 750°C at rate of 5-15 K/min in air flow; gas chromy., X-ray diffraction anal.;
参考文献
Derlyukova; Evdokimov
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 9 p. 1319 - 1322
in solid
Kinetics; applying satd. aq. soln. of CaCl2 to SiO2, evapn. of water, drying at 250°C to constant weight, kinetic study by gravimetric method, heating to ca. 850°C at rate of 5-15 K/min in air flow; gas chromy., X-ray diffraction anal.;
参考文献
Derlyukova; Evdokimov
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 9 p. 1319 - 1322
in gaseous matrix
byproducts: aluminium chloride oxide; gaseous AlCl3 carried by stream of Ar to react. zone held at 400-600°C, simultaneously stream of O2 contg. 2-5 vol percent H2O introduced into react. zone, react. allowed to proceed for 2 h; chem. and X-ray anal.;
参考文献
Shoji; Matsuzaki; Saeki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 437 - 440
