80937-33-3合成路线 (共 1249 条)
反应条件
T=700°C; KineticsThermodynamic data; Temperature;
参考文献
Borshchev; D'Yachenko; Kiselev; Kraidenko
Russian Journal of Applied Chemistry, 2013 , vol. 86, # 4 p. 493 - 497
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), 2013 , vol. 86, # 4 p. 530 - 534,5
反应条件
catalyst: trifluoroacetic acid in 1,4-dioxane Kinetics; byproducts: H2O, CO, CO2; Fe-complex oxidized in dioxane at 50°C with CF3CO2H;
参考文献
Fomin; Shirokov
Russian Journal of General Chemistry, 2011 , vol. 81, # 1 p. 81 - 90
反应条件
CF3COOH in dioxane Kinetics; Fe complex was kept in dioxane in the presence of acid in atm. of O2 at 50°C; not isolated; monitored by UV spectroscopy;
参考文献
Fomin; Shirokov
Russian Journal of General Chemistry, 2009 , vol. 79, # 11 p. 2304 - 2316
反应条件
in ethanol Kinetics; Fe complex was kept in EtOH in atm. of O2 at 50°C; not isolated; monitored by UV spectroscopy;
参考文献
Fomin; Shirokov
Russian Journal of General Chemistry, 2009 , vol. 79, # 11 p. 2304 - 2316
反应条件
in 1,4-dioxane Kinetics; Fe-complex oxidized in dioxane at 50°C;
参考文献
Fomin; Shirokov
Russian Journal of General Chemistry, 2011 , vol. 81, # 1 p. 81 - 90
参考文献
Inorganic Chemistry, , vol. 5, p. 1329 - 1333
Journal of Physical Chemistry, , vol. 69, p. 3160 - 3164
Diss. Cornell Univ. 1965
反应条件
in neat (no solvent) byproducts: O(BHO)2; oxidation:;
参考文献
Inorganic Chemistry, , vol. 5, p. 1329 - 1333
反应条件
in benzene-d6 P=760 Torr; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Tsvetkov, Nikolay P.; Andino, Jose G.; Fan, Hongjun; Verat, Alexander Y.; Caulton, Kenneth G.
Dalton Transactions, 2013 , vol. 42, # 19 p. 6745 - 6755
反应条件
in neat (no solvent) As2O3 added into large excess of PCl3 under N2, heated at 50-60°C with vigorous stirring for 7 h / slight amts. of O2 contained in app.; ppt. sepd., washed with PCl3, soln. distd. (667 Pa, 40°C); NMR anal.;
参考文献
Watanabe, Makoto; Van Wazer, John R.
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, p. 2902 - 2905
反应条件
in neat (no solvent) PbS annealed in oxygen atmosphere above 900 K; air quenched to room temp.; detd. by X-ray diffraction and X-ray photoelectron spectroscopy;
参考文献
Kamchatka; Chashchinov; Chesnokova
Inorganic Materials, 2001 , vol. 37, # 9 p. 910 - 914