80937-33-3合成路线 (共 1249 条)
反应条件
high charge of the sulfide;
参考文献
Gmelin Handbook: S: MVol.A2, 2.3.1, page 286 - 300
反应条件
methylene blue; N-ethyl-N,N-diisopropylamine in water; acetonitrile T=20°C; 7 h; Schlenk techniqueIrradiation;
参考文献
Pitre, Spencer P.; McTiernan, Christopher D.; Ismaili, Hossein; Scaiano, Juan C.
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13286 - 13289
反应条件
byproducts: Na2SO4, SO2; information about the react. eqs. in detail; react. with NaCl between 285 and 290°C, oxidn. of FeCl2 to FeCl3 at 350°C in presence of O2;
参考文献
Gmelin Handbook: Cu: MVol.A1, 3.6.2, page 423 - 446
反应条件
Kinetics; Irradiation (UV/VIS); photochemical oxidn., ambient temp.;
参考文献
Journal of Physical Chemistry, , vol. 70, p. 3008
C: MVol.D3, 2.1.1.10, page 19 - 20
反应条件
Kinetics; Irradiation (UV/VIS); photochemical oxidn., ambient temp.;
参考文献
Journal of Physical Chemistry, , vol. 70, p. 3008
C: MVol.D3, 2.1.1.10, page 19 - 20
反应条件
in neat (no solvent) reaction in a Pt vessel with air at high temperature;;
参考文献
Gmelin Handbook: Si: MVol.B, 47, page 121 - 123
反应条件
in gas Irradiation (UV/VIS); on photolysis (>= 300nm) of a Cl2-SiHCl3-N2-O2-mixture (0.2 Torr Cl2, 2Torr O2, 0.1 Torr SiHCl3, 700 Torr N2);; not isolated, monitoring of react. by IR;;
参考文献
Niki, H.; Maker, P. D.; Savage, C. M.; Breitenbach, L. P.; Hurley, M. D.
Journal of Physical Chemistry, 1985 , vol. 89, # 17 p. 3725 - 3729
反应条件
in gas Irradiation (UV/VIS); on photolysis (>= 300nm);; not isolated, monitoring of react. by IR (assignment proved by (15)N-labeling);;
参考文献
Niki, H.; Maker, P. D.; Savage, C. M.; Breitenbach, L. P.; Hurley, M. D.
Journal of Physical Chemistry, 1985 , vol. 89, # 17 p. 3725 - 3729
反应条件
in N,N-dimethyl-formamide Electrochem. Process; electrochemical generation of O2(1-) from O2 supplied to the cathode compartment (H-cell, DMF, supporting electrolyte (C4H9)4NPF6); pouring catholyte (with excess O2(1-)) into a flask containing flourene; bubbling O2, 10min, dark;; diln. of catholyte with H2O; extn. with diethyl ether; drying; removal of solvent, vac.; column chromy. (silica gel; eluent: hexane/CH2Cl2 (50percent));;
参考文献
Journal of Organometallic Chemistry, , vol. 273, # 3 p. 319 - 322
反应条件
sodium hydroxide in melt heating NaNO2 and NaOH to about 300°C until one of the components melts, oxidation by passing O2 (or air) through the soln.;;
参考文献
Gmelin Handbook: Na: SVol.1, 18, page 106 - 108
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I.G. Farbenindustrie A.-G.
Patent: GB306998 , 1929 ;
C. I, 1929 , p. 3024