80937-33-3合成路线 （共 1249 条）
反应条件
in gaseous matrix in Ar; various ratios Ar:B2H6 and Ar:O2; pyrolysis at 150-350°C; matrix isolation, IR;
参考文献
Barton, L.; Grimm, F. A.; Porter, R. F.
Inorganic Chemistry, 1966 , vol. 5, p. 2076 - 2078
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Porter, R. F.; Grimm, F. A.
Advances in Chemistry Series, 1968 , vol. 72, p. 94 - 100
反应条件
in gas byproducts: H2; pressure <40Torr, thermal, electrical or photochemical ignition of gas mixture;;
参考文献
Gmelin Handbook: B: B-Verb.13, 4.2, page 140 - 144
反应条件
in neat (no solvent) reaction at low pressure;;
参考文献
Gmelin Handbook: B: B-Verb.7, 3.1.3, page 17 - 19
反应条件
merged jet copyrolysis of Ar/B2H6 with Ar/O2 followed by trapping into an argon matrix (14 K); IR spectroscopic monitoring;
参考文献
Carpenter, John D.; Ault, Bruce S.
Journal of Molecular Structure, 1994 , vol. 319, p. 139 - 144
反应条件
in gaseous matrix other Radiation; ac discharge in a mixt. of BF3, O2, and He (partial pressure of BF3, O2, and He 60, 290, and 750 mTorr, dry-ice temp.);; detd. by diode laser spectroscopy and by microwave spectroscopy;;
参考文献
Kawashima, Yoshiyuki; Kawaguchi, Kentarou; Endo, Yasuki; Hirota, Eizi
Journal of Chemical Physics, 1987 , vol. 87, # 4 p. 2006 - 2009
反应条件
in gaseous matrix Kinetics; Ar as inert diluent gas, 675-1033 K, pressure was between 5.5 and 12.0 Torr; detected by fluorescence spectroscopy on basis of BF;
参考文献
Light, G. C.; Herm, R. R.; Matsumoto, J. H.
Journal of Physical Chemistry, 1985 , vol. 89, p. 5066 - 5074
反应条件
[Fe(dnbpn)(OTf)2] in acetonitrile T=24.84°C; Reagent/catalyst;
参考文献
Zhang, Qiao; Gorden, John D.; Goldsmith, Christian R.
Inorganic Chemistry, 2013 , vol. 52, # 23 p. 13546 - 13554
反应条件
in gas reacted in gas phase at 100-1100°C using F2 contg. ca. 1percent O2; further products; not isolated, detected by IR in Ar matrice;
参考文献
Osin; Davlyatshin; Ogden
Russian Journal of Physical Chemistry A, 2001 , vol. 75, # 2 p. 237 - 245
反应条件
in gas reacted in gas phase at 100-1100°C using F2 contg. ca. 1percent O2; further products; not isolated, detected by IR in Ar matrice;
参考文献
Osin; Davlyatshin; Ogden
Russian Journal of Physical Chemistry A, 2001 , vol. 75, # 2 p. 237 - 245
参考文献
Ye, Liqun; Liu, Xiaodi; Zhao, Qiang; Xie, Haiquan; Zan, Ling
Journal of Materials Chemistry C, 2013 , vol. 1, # 31 p. 8978 - 8983
