80937-33-3合成路线 （共 1249 条）
反应条件
in neat (no solvent, solid phase) suspn. of acetate in water was refluxed for 3 h, droplets of soln. were flash frozen by spraying on liquid N2, then freeze-dried, solid was heated at 773 K at rate of 5 K/min and held for 6 h under flowing O2; solid was allowed to cool inside the furnace; XRD;
参考文献
Villanueva, Regina; Gomez, Andres; Burguete, Pedro; Martinez, Eduardo; Beltran, Aurelio; Sapina, Fernando; Vicent, Monica; Sanchez, Enrique
Journal of the American Ceramic Society, 2011 , vol. 94, # 1 p. 237 - 244
反应条件
in neat (no solvent, gas phase) byproducts: Cl2; gaseous AlCl3 (formed by AlCl3 heating at 150°C) introduction toreaction zone by stream of Ar, dried O2 introduction, reaction for 2 h at 900 or 950°C, product ratio depends on temp., very low percent of reacted AlCl3 at temp. < 700°C; heating in Ar stream at 250°C, refluxing in ethanol with stirring for 2 h, centrifugation, repeated refluxing until Cl absence in ethanol phase, X-ray anal.;
参考文献
Shoji, Yuichi; Tatsumii, Kimikazu; Matsuzaki, Ryoko; Saeki, Yuzo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 1 p. 269 - 270
反应条件
in neat (no solvent) at 400°C in dry O2;
参考文献
Mittov; Ponomareva; Mittova
Inorganic Materials, 2002 , vol. 38, # 5 p. 438 - 444
反应条件
in solid Kinetics; in air at 800-1100°C; XRD, SEM;
参考文献
Barsoum; Tzenov; Procopio; El-Raghy; Ali
Journal of the Electrochemical Society, 2001 , vol. 148, # 8 p. C551-C562
反应条件
in solid Kinetics; in air at 800-1100°C; XRD, SEM;
参考文献
Barsoum; Tzenov; Procopio; El-Raghy; Ali
Journal of the Electrochemical Society, 2001 , vol. 148, # 8 p. C551-C562
反应条件
in solid Kinetics; in air at 800-1100°C; XRD, SEM;
参考文献
Barsoum; Tzenov; Procopio; El-Raghy; Ali
Journal of the Electrochemical Society, 2001 , vol. 148, # 8 p. C551-C562
反应条件
in neat (no solvent, solid phase) heating under air to 700°C; mass spectrometry;
参考文献
Prevot; Forano; Besse
Journal of Solid State Chemistry, 2000 , vol. 153, # 2 p. 301 - 309
反应条件
in neat (no solvent) TG-DTA in oxygen atm. in range between 25 - 700 °C at heating rate of 10 °C/min, decompd. at 580°C;
参考文献
Paljevic M.
Journal of the Less-Common Metals, 1990 , vol. 157, p. 289 - 294
反应条件
in neat (no solvent) heated at heating rate of 1°C/s to 700°C in 80percent N2/20percent O2 gas flow mixt.;
参考文献
Morgan, Alexander B.; Wolf, J. Douglas; Guliants, Elena A.; Fernando, K.A. Shiral; Lewis, William K.
Thermochimica Acta, 2009 , vol. 488, # 1-2 p. 1 - 9
反应条件
in neat (no solvent) Kinetics; mixed, combusted in oxy-acetylene flame; DTA, EDS;
参考文献
Hasani; Panjepour; Shamanian
Journal of Alloys and Compounds, 2010 , vol. 502, # 1 p. 80 - 86
