反应条件
1: 96 percent / DMAP / acetonitrile / 24 h 2: 89 percent / H2 / Pd/C / methanol / 2 h / 2585.74 Torr 3: Et3N / tetrahydrofuran / 0.5 h / -10 °C 4: tetrahydrofuran; H2O / 1.5 h / -10 °C 5: 2.52 g / toluene / 2 h / Heating 6: 95 percent / CuCl / dimethylformamide / 1 h 7: 10 percent / NaOH / methanol; H2O / 2 h View Scheme
参考文献
Englund, Ethan A.; Gopi, Hosahudya N.; Appella, Daniel H.
Organic Letters, 2004 , vol. 6, # 2 p. 213 - 215
