1,4,5,8-萘四甲酸酐合成路线 （共 53 条）
反应条件
1.1: sulfuric acid, fuming / 2 h / 55 °C 1.2: 50 h / 85 °C 2.1: propionic acid / o-xylene / 2 h / 140 °C 3.1: zinc; acetic acid / isopropyl alcohol; water / 90 °C / |Inert atmosphere View Scheme
参考文献
Steyrleuthner, Robert; Di Pietro, Riccardo; Collins, Brian A.; Polzer, Frank; Himmelberger, Scott; Schubert, Marcel; Chen, Zhihua; Zhang, Shiming; Salleo, Alberto; Ade, Harald; Facchetti, Antonio; Neher, Dieter
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4245 - 4256
反应条件
1: naphthalene-1,4,5,8-tetracarboxylic acid dianhydride With sulfuric acid; dibromoisocyanuric acid 2: 2-decyltetradecylamine With acetic acid T=120°C; Inert atmosphere;
参考文献
Guo, Xugang; Watson, Mark D.
Organic Letters, 2008 , vol. 10, # 23 p. 5333 - 5336
反应条件
potassium hydroxide pH=6.4;
参考文献
Barros; Cuccovia; Farah; Masini; Chaimovich; Politi
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 1 p. 71 - 82
反应条件
ammonium hydroxide T=20°C; 6 h;
参考文献
Kacprzak, Karol
Synthetic Communications, 2003 , vol. 33, # 9 p. 1499 - 1507
参考文献
Bamberger; Philip
Justus Liebigs Annalen der Chemie, 1887 , vol. 240, p. 185
反应条件
zinc diacetate in N-methyl-1,2-pyrrolidone 5 h; Heating / reflux;
参考文献
Xerox Corporation
Patent: EP1795532 A1, 2007 ;
Location in patent: Page/Page column 20-21 ;
反应条件
zinc diacetate T=250°C; 3 h; Neat (no solvent);
参考文献
Mamada, Masashi; Perez-Bolivar, Cesar; Anzenbacher, Pavel
Organic Letters, 2011 , vol. 13, # 18 p. 4882 - 4885
反应条件
in tetrahydrofuran 8 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 9, # 8 p. 2015 - 2024
反应条件
in isopropyl alcohol Heating;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 9, # 9 p. 2329 - 2334
反应条件
pyridine; zinc diacetate Heating;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 9, # 9 p. 2329 - 2334
