1,4,5,8-萘四甲酸酐合成路线 （共 53 条）
反应条件
sulfuric acid; sulfur trioxide; bromine; iodine T=140°C; 672000 h;
参考文献
Gao, Xike; Qiu, Wenfeng; Yang, Xiaodi; Liu, Yunqi; Wang, Ying; Zhang, Hengjun; Qi, Ting; Liu, Ying; Lu, Kun; Du, Chunyan; Shuai, Zhigang; Yu, Gui; Zhu, Daoben
Organic Letters, 2007 , vol. 9, # 20 p. 3917 - 3920
反应条件
sulfuric acid; dibromoisocyanuric acid Title compound not separated from byproducts.;
参考文献
Kishore, Ravuri S. K.; Ravikumar, Velayutham; Bernardinelli, Gerald; Sakai, Naomi; Matile, Stefan
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 738 - 740
反应条件
bromine Product distribution;
参考文献
Solomatin, G. G.; Filippov, M. P.; Shigalevskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 771 - 773
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 877 - 879
反应条件
1: naphthalene-1,4,5,8-tetracarboxylic acid dianhydride With sulfuric acid T=85°C; 0.5 h; 2: With potassium 1,3-dibromoisocyanurate T=85°C; 20 h; 3: 1-Hexylamine With acetic acid 0.333333 h; Reflux; TimeConcentration;
参考文献
INSTITUTE OF CHEMISTRY, CHINESE ACADEMY OF SCIENCES; WANG, Zhaohui; YUE, Wan
Patent: WO2013/91279 A1, 2013 ;
Location in patent: Page/Page column 32 ;
反应条件
1: sulfuric acid; potassium 1,3-dibromoisocyanurate / 48 h / 85 °C 2: acetic acid / 0.33 h / Reflux View Scheme
参考文献
GEORGIA TECH RESEARCH CORPORATION; POLANDER, Lauren, E.; TIWARI, Shree, Prakash; MARDER, Seth; KIPPELEN, Bernard; DASARI, Raghunath, R.; GETMANENKO, Yulia, A.; HWANG, Do Kyung; FENOLL, Mathieu
Patent: WO2012/142460 A1, 2012 ;
反应条件
in acetone carbon deposition on LiFePO4 substrate; dispersion of ground LiFePO4 in soln. of org. compd. in acetone evapd., residue heated in a stream of CO2/CO gas, heated to 650°C in 100 min, kept at final temp. for 1 h, cooling; XRD;
参考文献
Journal of the Electrochemical Society, , vol. 157, # 4 p. A453-A462
反应条件
potassium hydroxide in methanol; dimethyl sulfoxide 0.5 h; Ambient temperature;
参考文献
Acton, Nancy; Hou, Donald; Schwarz, Joshua; Katz, Thomas J.
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1011 - 1018
反应条件
2-Methylpropanedioic Acid Ethyl Methyl Ester; zinc(II) chloride T=180°C; Erhitzen des Reaktionsprodukts mit wss. HI und rotem Phosphor bis auf 200grad und Erhitzen des hierbei erhaltenen Reaktionsprodukts mit Kupfer auf 500grad;
参考文献
Runge; Meckelburg
Chemische Berichte, 1953 , vol. 86, p. 373,376
反应条件
1: naphthalene-1,4,5,8-tetracarboxylic acid dianhydride With sulfuric acid T=85°C; 0.5 h; 2: With potassium 1,3-dibromoisocyanurate T=85°C; 20 h; 3: 1-Hexylamine With acetic acid 0.333333 h; Reflux; TimeConcentration;
参考文献
WO2013/91279 A1, ;
Page/Page column 32 ;
反应条件
1.1: sulfuric acid, fuming / 2 h / 55 °C 1.2: 50 h / 85 °C 2.1: propionic acid / o-xylene / 2 h / 140 °C View Scheme
参考文献
Steyrleuthner, Robert; Di Pietro, Riccardo; Collins, Brian A.; Polzer, Frank; Himmelberger, Scott; Schubert, Marcel; Chen, Zhihua; Zhang, Shiming; Salleo, Alberto; Ade, Harald; Facchetti, Antonio; Neher, Dieter
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4245 - 4256
