1,4,5,8-萘四甲酸酐合成路线 （共 53 条）
反应条件
sulfuric acid; bromine; iodine
参考文献
Nakatsuji, Shin'ichi; Aoki, Kazunori; Akutsu, Hiroki; Yamada, Jun-Ichi; Kojima, Takahiro; Nishida, Jun-Ichi; Yamashita, Yoshiro
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 9 p. 1079 - 1085
反应条件
1: 77 percent / KOH / dimethylsulfoxide; methanol / 0.5 h / Ambient temperature
2: 1.) diisobutylaluminum hydride / toluene / 1.) reflux, 10 h, 2.) room temp., 6 h
3: 79 percent / PBr3, tetra-n-butylammonium bromide / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Acton, Nancy; Hou, Donald; Schwarz, Joshua; Katz, Thomas J.
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1011 - 1018
反应条件
sulfuric acid; dibromoisocyanuric acid
T=130°C; 15 h;
参考文献
Chaignon, Frederique; Falkenstroem, Magnus; Karlsson, Susanne; Blart, Errol; Odobel, Fabrice; Hammarstroem, Leif
Chemical Communications, 2007 , # 1 p. 64 - 66
反应条件
1: With sulfuric acid; sulfur trioxide
3 h;
2: With iodine
1 h;
3: With bromine
T=95°C; 24.25 h;
参考文献
INSTITUTE OF CHEMISTRY, CHINESE ACADEMY OF SCIENCES; WANG, Zhaohui; YUE, Wan
Patent: WO2013/91279 A1, 2013 ;
Location in patent: Page/Page column 32 ;
反应条件
sulfuric acid; sulfur trioxide; dibromoisocyanuric acid
5 h;
参考文献
BASF SE
Patent: US2008/300405 A1, 2008 ;
Location in patent: Page/Page column 17-18 ;
反应条件
oleum (20percent SO3)
T=40°C; 5 h;
参考文献
Ma, Lihua; Guo, Song; Sun, Jifu; Zhang, Caishun; Zhao, Jianzhang; Guo, Huimin
Dalton Transactions, 2013 , vol. 42, # 18 p. 6478 - 6488
反应条件
sulfuric acid; dibromoisocyanuric acid
Title compound not separated from byproducts.;
参考文献
Kishore, Ravuri S. K.; Ravikumar, Velayutham; Bernardinelli, Gerald; Sakai, Naomi; Matile, Stefan
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 738 - 740
反应条件
bromine
Product distribution;
参考文献
Solomatin, G. G.; Filippov, M. P.; Shigalevskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 771 - 773
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 877 - 879
反应条件
SnCl2·2H2O; zinc diacetate; propionic acid
8 h; Inert atmosphereReflux;
参考文献
Xiong, Kai; Xiao, Yi
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3171 - 3175
反应条件
zinc diacetate
T=250°C; 3 h; Neat (no solvent);
参考文献
Mamada, Masashi; Perez-Bolivar, Cesar; Anzenbacher, Pavel
Organic Letters, 2011 , vol. 13, # 18 p. 4882 - 4885
