4-溴-1,8-萘二甲酸酐合成路线 （共 43 条）
反应条件
in 3-methyl-1-butanol T=132°C; 12 h;
参考文献
Plakidin, Val. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 5 p. 990 - 991
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1118 - 1119
反应条件
in 3-methyl-1-butanol T=132°C; 50 h;
参考文献
Plakidin, Val. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 5 p. 990 - 991
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1118 - 1119
反应条件
in 3-methyl-1-butanol T=130°C; 15 h; other solvent; other temperature; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 2273 - 2281
Zhurnal Organicheskoi Khimii, , vol. 19, # 12 p. 2591 - 2600
反应条件
1: Hydrolysis.anschliessend Umsetzen mit Diazomethan 2: benzene; diethyl ether; LiAlH4 3: benzene; diethyl ether; PBr3 4: benzene View Scheme
参考文献
Bergmann; Szmuszkovicz
Journal of the American Chemical Society, 1953 , vol. 75, p. 2760
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1754 - 1755
Zhurnal Organicheskoi Khimii, , vol. 18, # 9 p. 1997 - 1998
反应条件
1,4-diaza-bicyclo[2.2.2]octane in dimethyl sulfoxide T=20 - 28°C; Inert atmosphere;
参考文献
Murai, Toshihiko; Makabe, Yoshie; Fujita, Shohei
Patent: US2012/289697 A1, 2012 ;
Location in patent: Page/Page column 21 ;
反应条件
bei der Destillation;
参考文献
Graebe; Guinsbourg
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 86
反应条件
1.1: NaOH; Cu / dimethylformamide / 1 h / Heating 2.1: Fe; AcOH / 1 h / Heating 3.1: aq. HCl; NaNO2; AcOH / 1 h / 0 - 5 °C 3.2: aq. CuSO4; AcOH / 0.5 h / Heating View Scheme
参考文献
Yin, Hong; Zhu, Weiping; Xu, Yufang; Dai, Min; Qian, Xuhong; Li, Yuanli; Liu, Jianwen
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 7 p. 3030 - 3037
反应条件
1: With sodium hydroxide Heating; 2: With mercury(II) oxide in water; acetic acid 96 h; Heating; 3: With hydrogenchloride 3 h; Heating;
参考文献
Li, Zhigang; Yang, Qing; Qian, Xuhong
Tetrahedron, 2005 , vol. 61, # 36 p. 8711 - 8717
反应条件
1.1: 77 percent / K2CO3 / dimethylformamide / 0.5 h / Heating 2.1: sodium nitrite; HCl; acetic acid / H2O / 0.33 h / 0 - 5 °C 2.2: 99 percent / CuSO4; acetic acid / H2O / 1.5 h / Heating View Scheme
参考文献
Qian, Xuhong; Li, Yonggang; Xu, Yufang; Liu, Yan; Qu, Baoyuan
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 10 p. 2665 - 2668
