trichlorophosphate in 1,2-dichloro-ethane T=0 - 85°C; 5.25 h; Inert atmosphere;
参考文献
Czaplyski, William L.; Purnell, Grace E.; Roberts, Courtney A.; Allred, Rebecca M.; Harbron, Elizabeth J.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 3 p. 526 - 533
1: With 4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 4 h; Inert atmosphereDarkness; 2: With hydrogenchloride in dichloromethane; water
