反应条件
1.1: sodium iodide / butanone / 22 h / 80 °C 2.1: zinc; water; hydrogenchloride / ethanol / 19 h / 10 - 24 °C 3.1: sodium carbonate; magnesium sulfate / ethanol; water / 23 h / 25 °C 4.1: toluene / 5 h / |Reflux 5.1: zinc; acetic acid / diethyl ether / 72 h / 0 - 25 °C 5.2: pH 7.2 6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / |Inert atmosphere 6.2: 4 h / 0 - 20 °C / |Inert atmosphere 7.1: hydrogenchloride / water / 7 h / 20 °C 8.1: hydrogen; palladium 10 on activated carbon / methanol / 16 h / 7500.75 Torr 9.1: triethylamine / 48 h / 75 °C 10.1: water; acetic acid; sodium nitrite / 20 h / 25 °C 11.1: O-(6-chloro-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 25 °C / |Inert atmosphere 11.2: 16 h / 25 °C / |Inert atmosphere View Scheme
